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1-Bromo-9H-carbazole

CAS No.
16807-11-7
Chemical Name:
1-Bromo-9H-carbazole
Synonyms
1-broMocarbazole;1-bromo-9H-carbozle;-broMo-9H-carbazole;-broMo-9H-carbazole;1-Bromocarbazole >1-broMo-9H-carbazole;9H-Carbazole, 1-broMo-
CBNumber:
CB22595627
Molecular Formula:
C12H8BrN
Molecular Weight:
246.1
MDL Number:
MFCD18450164
MOL File:
16807-11-7.mol
MSDS File:
SDS
Last updated:2023-12-22 17:53:22

1-Bromo-9H-carbazole Properties

Melting point 123-124℃ (acetic acid )
Boiling point 409.2±18.0 °C(Predicted)
Density 1.617±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
form powder to crystal
pka 16.14±0.30(Predicted)
color White to Light yellow

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313
HS Code  2933998090

1-Bromo-9H-carbazole price More Price(34)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical B4816 1-Bromocarbazole >98.0%(GC) 16807-11-7 200mg $34 2024-03-01 Buy
TCI Chemical B4816 1-Bromocarbazole >98.0%(GC) 16807-11-7 1g $97 2024-03-01 Buy
TRC B678900 1-Bromo-9H-carbazole 16807-11-7 5mg $60 2021-12-16 Buy
TRC B678900 1-Bromo-9H-carbazole 16807-11-7 25mg $75 2021-12-16 Buy
SynQuest Laboratories 3H31-9-1C 1-Bromo-9H-carbazole 99% 16807-11-7 25g $493 2021-12-16 Buy
Product number Packaging Price Buy
B4816 200mg $34 Buy
B4816 1g $97 Buy
B678900 5mg $60 Buy
B678900 25mg $75 Buy
3H31-9-1C 25g $493 Buy

1-Bromo-9H-carbazole Chemical Properties,Uses,Production

Chemical Properties

White to yellow powder or crystals.

Uses

1-Bromo-9H-carbazole is a useful research chemical, mainly used as a pharmaceutical intermediate and an intermediate in organic synthesis.

Preparation

A 1-Bromo-9H-carbazole is synthesized as follows:Under noble gas protection, by 3,6- bis- Tert-butyl carbazole is dissolved in 1,2- dichloroethanes, adds hydrobromic acid, controlling reaction temperature to be slowly added dropwise hydrogen peroxide, dropping is completely Overnight, reactant liquor is washed, and separates organic layer for natural temperature reaction, is dried, and adds methyl alcohol dispersion, obtains the tertiary fourth of bromo- 3, the 6- of 1- bis- Base carbazole;Then 1- bromo- 3,6- di-t-butyl carbazole and isopropanol solvent are added in reaction bulb, controlling reaction temperature slowly adds Enter alchlor reaction, add water after terminating terminating reaction, through extraction, organic layer sodium hydrate aqueous solution is washed, and is dried overnight, concentrate Obtain crude product, methylene chloride-methanol mixed solvent is recrystallized to give product 1-Bromo-9H-carbazole.
Production method of 1-bromocarbazole

Definition

1-Bromo-9H-carbazole is a bromide-substitution of carbazole. The carbazole ring system is essentially planar (r.m.s. deviation of 0.024? for the non-H atoms). It is a photoelectric material intermediate and be used to synthesize OLED materials.

86-74-8
16807-11-7
Synthesis of 1-Bromo-9H-carbazole from Carbazole

1-Bromo-9H-carbazole Preparation Products And Raw materials

Raw materials

Preparation Products

Global( 214)Suppliers
Supplier Tel Email Country ProdList Advantage
Siyang Liaoning Biochemical Products Co. Ltd
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Jiangsu Nata Opto-electronic Material Co.,Ltd.
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Hebei Xinsheng New Material Technology Co., LTD.
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Henan Fengda Chemical Co., Ltd
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Springchem New Material Technology Co.,Limited
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Capot Chemical Co.,Ltd.
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Nanjing ChemLin Chemical Industry Co., Ltd.
025-83697070 product@chemlin.com.cn CHINA 3012 60

View Lastest Price from 1-Bromo-9H-carbazole manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1-Bromocarbazole pictures 2024-06-07 1-Bromocarbazole
16807-11-7
US $0.00-0.00 / kg 1kg 98%+ 1000kg per Month Shanghai Qyubiotech Co., Ltd.
9H-Carbazole, 1-bromo- pictures 2024-01-23 9H-Carbazole, 1-bromo-
16807-11-7
US $0.00 / KG 1KG 98.00% 150KG /month Shanghai Daken Advanced Materials Co.,Ltd
1-Bromo-9H-carbazole pictures 2023-12-23 1-Bromo-9H-carbazole
16807-11-7
US $50.00-1.00 / KG 1KG 99% g-kg-tons, free sample is available Henan Fengda Chemical Co., Ltd

1-Bromo-9H-carbazole Spectrum

-broMo-9H-carbazole 1-broMo-9H-carbazole 9H-Carbazole, 1-broMo- 1-bromo-9H-carbozle 1-Bromocarbazole > -broMo-9H-carbazole 1-broMocarbazole 16807-11-7