1,2-Bis(maleimido)ethane synthesis
- Product Name:1,2-Bis(maleimido)ethane
- CAS Number:5132-30-9
- Molecular formula:C10H8N2O4
- Molecular Weight:220.18
32620-84-1
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5132-30-9
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$67.20/25MG
Yield:5132-30-9 85%
Reaction Conditions:
in 1,1,2,2-tetrachloroethane at 120; for 12 h;
Steps:
General procedure for retro-Diels-Alder reaction
General procedure: A solution of alkylated product(1 mol) in 1,1,2,2-tetrachloroethane was stirred at 120 C in an open flask for12 h. After completion of the reaction as indicated by TLC, the solvent wasevaporated under reduced pressure to afford BMI.
References:
Rao, Venkataramanarao;Navath, Suryakiran;Kottur, Mohankumar;McElhanon, James R.;McGrath, Dominic V. [Tetrahedron Letters,2013,vol. 54,# 37,p. 5011 - 5013]
55750-48-6
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107-15-3
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5132-30-9
102 suppliers
$67.20/25MG
108-31-6
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$13.47/50g
125923-10-6
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$105.00/50mg
5132-30-9
102 suppliers
$67.20/25MG
7126-27-4
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$62.00/250mg
5132-30-9
102 suppliers
$67.20/25MG
108-31-6
835 suppliers
$13.47/50g
107-15-3
9 suppliers
$11.19/25ML
5132-30-9
102 suppliers
$67.20/25MG