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ChemicalBook CAS DataBase List 1H,1H-PERFLUORO-1-HEPTANOL

1H,1H-PERFLUORO-1-HEPTANOL synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 86 percent / O3/O2 / 1,1,2-trichloro-1,2,2-trifluoro-ethane; methanol / 2 h / 0 - 5 °C
2: 70 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C

References:

Odinokov;Akhmetova;Bazunova;Savchenko;Paramonov;Khalilov [Russian Journal of Organic Chemistry,2001,vol. 37,# 3,p. 321 - 325]

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