2-(4-METHYLTHIOPHENYL)PYRIDINE synthesis
- Product Name:2-(4-METHYLTHIOPHENYL)PYRIDINE
- CAS Number:4373-59-5
- Molecular formula:C12H11NS
- Molecular Weight:201.29
Yield:4373-59-5 156 mg
Reaction Conditions:
Stage #1: 2-bromo-pyridinewith isopropylmagnesium chloride in tetrahydrofuran at 20; for 4 h;Inert atmosphere;Cooling with ice;
Stage #2: with zinc(II) chloride in tetrahydrofuran at 20; for 2 h;Inert atmosphere;Cooling with ice;
Stage #3: (4-bromophenyl)thioanisoleFurther stages;
References:
Colombe, James R.;Bernhardt, Sebastian;Stathakis, Christos;Buchwald, Stephen L.;Knochel, Paul [Organic Letters,2013,vol. 15,# 22,p. 5754 - 5757] Location in patent:supporting information
109-04-6
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190788-58-0
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4373-59-5
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$481.00/1g
1778-09-2
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109-76-2
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4373-59-5
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109-04-6
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98546-51-1
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4373-59-5
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5188-07-8
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4373-59-5
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