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2,5-Dimethyl-2-phenyl-4-hexal synthesis

2synthesis methods
-

Yield:1015-18-5 68%

Reaction Conditions:

Stage #1: 2-Phenylpropanalwith sodium hydride in tetrahydrofuran at 20; for 0.5 h;
Stage #2: prenyl bromide in tetrahydrofuran at 20; for 0.5 h;

References:

Foerster, Bettina;Bertermann, Ruediger;Kraft, Philip;Tacke, Reinhold [Organometallics,2014,vol. 33,# 1,p. 338 - 346]