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ChemicalBook CAS DataBase List 2-Amino-3,4-dimethylbenzoic acid

2-Amino-3,4-dimethylbenzoic acid synthesis

5synthesis methods
69272-50-0 Synthesis
3,6-dibroMo-1,2-BenzenediaMine

69272-50-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: Na2SO4, hydroxylamine sulfate, concd. HCl / H2O
2: 65 percent / CH3SO3H / 70 - 80 °C
3: 65 percent / KOH, KCl, 27percent H2O2 / 20 °C

References:

Rewcastle, Gordon W.;Atwell, Graham J.;Zhuang, Li;Baguley, Bruce C.;Denny, William A. [Journal of Medicinal Chemistry,1991,vol. 34,# 1,p. 217 - 222]

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