2-BROMO-6-FLUOROANILINE synthesis
- Product Name:2-BROMO-6-FLUOROANILINE
- CAS Number:65896-11-9
- Molecular formula:C6H5BrFN
- Molecular Weight:190.01
2252-37-1
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$9.00/1g
65896-11-9
295 suppliers
$6.00/1g
Yield:65896-11-9 86%
Reaction Conditions:
Stage #1:2-bromo-6-fluorobenzoic acid with sulfuric acid at 60; for 1.5 h;
Stage #2: with sodium azide at 20; for 42 h;Schmidt rearrangement;
Stage #3: with ammonium hydroxide at 0;
References:
Morrison, Matthew D.;Hanthorn, Jason J.;Pratt, Derek A. [Organic Letters,2009,vol. 11,# 5,p. 1051 - 1054] Location in patent:supporting information; experimental part
348-54-9
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$10.00/1g
367-24-8
487 suppliers
$15.00/25 g
141474-37-5
161 suppliers
$10.00/1g
65896-11-9
295 suppliers
$6.00/1g
348-54-9
414 suppliers
$10.00/1g
65896-11-9
295 suppliers
$6.00/1g
348-54-9
414 suppliers
$10.00/1g
367-24-8
487 suppliers
$15.00/25 g
65896-11-9
295 suppliers
$6.00/1g