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ChemicalBook CAS DataBase List 2-TERT-BUTYLCYCLOHEXANONE

2-TERT-BUTYLCYCLOHEXANONE synthesis

10synthesis methods
-

Yield:-

Reaction Conditions:

with hydrogen at 59.84; under 4500.45 Torr; for 2 h;Catalytic behavior;Autoclave;Time;Pressure;

Steps:


The flask containing the reaction mixture was purged six times with hydrogen in order to remove air completely before being stirred vigorously under ordinary hydrogen atmosphere. A typical reaction was carried out in an autoclave batch reactor. After loading the reactant, catalyst and solvent, the reactor was flushed six times with H2. At 333 K and a stirring speed of 750 rpm, H2 was charged (1 or 6 bar) for 2 or 6 h..

References:

Li, Xinzheng;Cheng, Ling;Wang, Xingyi [Research on Chemical Intermediates,2019,vol. 45,# 3,p. 1249 - 1262]

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