3-N-Boc-amino-azetidine synthesis
- Product Name:3-N-Boc-amino-azetidine
- CAS Number:91188-13-5
- Molecular formula:C8H16N2O2
- Molecular Weight:172.22
91189-18-3
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$93.00/25 mg
91188-13-5
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$8.00/250mg
Yield:91188-13-5 100%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in ethanol at 20; for 2 h;
Steps:
1.1.A
A mixture of (113 mg, 0.33 mmol) and 10% Pd/C (88 mg) in ethanol (3 ml) was stirred under hydrogen atmosphere at rt for 2 h. The reaction mixture was filtered and evaporated to give XXA (63 mg) as a white solid.
References:
Bisacchi, Gregory S.;Sutton, James C.;Slusarchyk, William A.;Treuner, Uwe;Zhao, Guohua US2004/147502, 2004, A1 Location in patent:Page/Page column 23; 25