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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4-Fluoro-9H-fluoren-9-one synthesis

8synthesis methods
2'-fluoro-[1,1'-biphenyl]-2-carbonitrile

400820-15-7
1 suppliers
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4-Fluoro-9H-fluoren-9-one

1514-18-7
1 suppliers
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Yield:1514-18-7 46%

Reaction Conditions:

with dichloro bis(acetonitrile) palladium(II);water;silver trifluoroacetate in N,N-dimethyl acetamide;trifluoroacetic acid at 140; for 72 h;Glovebox;Inert atmosphere;Heck Reaction;

References:

Wan, Jung-Chih;Huang, Jun-Min;Jhan, Yu-Huei;Hsieh, Jen-Chieh [Organic Letters,2013,vol. 15,# 11,p. 2742 - 2745] Location in patent:supporting information

50-00-0 Synthesis
Formaldehyde

50-00-0
842 suppliers
$10.00/25g

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1554-05-8
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4-Fluoro-9H-fluoren-9-one

1514-18-7
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References
891180-59-9 Synthesis
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891180-59-9
106 suppliers
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98-80-6 Synthesis
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98-80-6
705 suppliers
$5.00/5g

4-Fluoro-9H-fluoren-9-one

1514-18-7
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References
1993-03-9 Synthesis
2-Fluorophenylboronic acid

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350 suppliers
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6630-33-7
406 suppliers
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4-Fluoro-9H-fluoren-9-one

1514-18-7
1 suppliers
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References
2-Cyanophenylboronic acid

138642-62-3
322 suppliers
$15.00/1g

4-Fluoro-9H-fluoren-9-one

1514-18-7
1 suppliers
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References