4-NITROSOANISOLE synthesis
- Product Name:4-NITROSOANISOLE
- CAS Number:1516-21-8
- Molecular formula:C7H7NO2
- Molecular Weight:137.14
5720-07-0
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Yield:1516-21-8 130 mg
Reaction Conditions:
Stage #1: 4-methoxybenzeneboronic acidwith potassium hydrogen difluoride in methanol;lithium hydroxide monohydrate at 0 - 20; for 0.0333333 h;Inert atmosphere;
Stage #2: with nitrosonium tetrafluoroborate in acetonitrile at 20; for 0.00833333 h;regioselective reaction;
References:
Molander, Gary A.;Cavalcanti, Livia N. [Journal of Organic Chemistry,2012,vol. 77,# 9,p. 4402 - 4413] Location in patent:experimental part
104-94-9
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100-66-3
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877-68-9
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100-17-4
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51437-65-1
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501-58-6
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