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5-(1-Naphtyl)-3-phenylisoxazole synthesis

6synthesis methods
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetra-(n-butyl)ammonium iodide; hydroxylamine hydrochloride / water / 5 h / Inert atmosphere; Reflux
2: toluene-4-sulfonic acid / water / 1 h / 20 °C

References:

Harigae, Ryo;Moriyama, Katsuhiko;Togo, Hideo [Journal of Organic Chemistry,2014,vol. 79,# 5,p. 2049 - 2058]