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5-broMo-2-iodo-biphenyl synthesis

2synthesis methods
-

Yield:4510-78-5 89%

Reaction Conditions:

with toluene-4-sulfonic acid;potassium iodide;sodium nitrite in acetonitrile at 10 - 20; for 2 h;

References:

Golling, Florian E.;Quernheim, Martin;Wagner, Manfred;Nishiuchi, Tomohiko;Muellen, Klaus [Angewandte Chemie - International Edition,2014,vol. 53,# 6,p. 1525 - 1528][Angew. Chem.,2014,vol. 126,# 6,p. 1551 - 1554,4] Location in patent:supporting information