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Pentacyclo[4.2.0.02,5.03,8.04,7]octane, 1,4-diiodo- synthesis

6synthesis methods
4-iodocubanecarboxylic acid

111873-46-2
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Pentacyclo[4.2.0.02,5.03,8.04,7]octane, 1,4-diiodo-

97229-08-8
3 suppliers
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Yield:97229-08-8 93%

Reaction Conditions:

with 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione in 1,2-dichloro-ethane; for 2 h;Irradiation;Inert atmosphere;Reflux;

References:

Kulbitski, Kseniya;Nisnevich, Gennady;Gandelman, Mark [Advanced Synthesis and Catalysis,2011,vol. 353,# 9,p. 1438 - 1442] Location in patent:supporting information; experimental part