BenzaMide, N-[2-(aMinocarbonyl)phenyl]-3-Methoxy- synthesis
- Product Name:BenzaMide, N-[2-(aMinocarbonyl)phenyl]-3-Methoxy-
- CAS Number:330657-87-9
- Molecular formula:C15H14N2O3
- Molecular Weight:270.28
Yield:330657-87-9 100%
Reaction Conditions:
with pyridine in chloroform at 20; for 6 h;
Steps:
1
To a solution of anthranilamide (7.0 g, 51.41 mmole) in CHCl3 (260 mL) was added pyridine (8.13 g, 102.8 mmole, 8.28 mL) followed by slow addition of w-anisoyl chloride (9.20 g, 53.94 mmole, 7.35 mL). The reaction mixture was stirred at ambient temperature for 6 h and then concentrated in vacuo and subsequently dried under high vacuum for 4 h to give the product. (13.89g, mmol, 100%)
References:
WO2008/54599,2008,A2 Location in patent:Page/Page column 104
![methyl 2-[(3-methoxybenzoyl)amino]benzoate](/CAS/20180720/GIF/67836-50-4.gif)
67836-50-4
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