Boc-3,4-dehydro-D-proline Methyl ester synthesis
- Product Name:Boc-3,4-dehydro-D-proline Methyl ester
- CAS Number:220652-51-7
- Molecular formula:C11H17NO4
- Molecular Weight:227.26
73286-70-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 83 percent / LDA / heptane; tetrahydrofuran; ethylbenzene / 1 h / 5 °C
2: NaHCO3; Novozyme 435 / H2O / 24 h / 50 °C / pH 6.5 - 8.5
References:
Stuermer;Schaefer;Wolfart;Stahr;Kazmaier;Helmchen [Synthesis,2001,# 1,p. 46 - 48]
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51154-06-4
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24424-99-5
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