METHYL 2,4-DIFLUOROBENZOATE synthesis
- Product Name:METHYL 2,4-DIFLUOROBENZOATE
- CAS Number:106614-28-2
- Molecular formula:C8H6F2O2
- Molecular Weight:172.13
67-56-1
733 suppliers
$9.00/25ml
72482-64-5
195 suppliers
$13.43/1gm:
106614-28-2
235 suppliers
$6.00/5g
Yield:106614-28-2 100%
Reaction Conditions:
at 20; for 2 h;
Steps:
6.1
To 100 mL of MeOH, 2,4-difluorobenzoyl chloride (10 mL, 79.3 mmol) was added and the mixture stirred at room temperature for 2 hours. The solvent was then evaporated affording the tilte compound as pale yellow oil (quantitative).IH-NMR (400 MHz), δ (ppm, DMSOtZ6): 8.0 (m, IH), 7.44 (m, IH), 7.25 (m, IH),3.87 (s, 3H).
References:
WO2007/68619,2007,A1 Location in patent:Page/Page column 97
1583-58-0
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$6.00/5g
106614-28-2
235 suppliers
$6.00/5g
67-56-1
733 suppliers
$9.00/25ml
1583-58-0
413 suppliers
$6.00/5g
106614-28-2
235 suppliers
$6.00/5g
124-38-9
122 suppliers
$214.00/14L
2265-93-2
219 suppliers
$8.00/5g
74-88-4
341 suppliers
$15.00/10g
106614-28-2
235 suppliers
$6.00/5g
367-27-1
328 suppliers
$6.00/5g
106614-28-2
235 suppliers
$6.00/5g