Testosterone phenylpropionate synthesis
- Product Name:Testosterone phenylpropionate
- CAS Number:1255-49-8
- Molecular formula:C28H36O3
- Molecular Weight:420.58
58-22-0
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$21.00/1mg
104-55-2
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$6.00/25g
1255-49-8
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$17.00/5mg
Yield:1255-49-8 64%
Reaction Conditions:
with 3-butyl-1-methylimidazolium acetate in 1,4-dioxane at 120; for 2 h;
Steps:
7
In a 100 ml reaction flask, 0.397 g (3 mmol) of cinnamaldehyde was added.0.411g (1.5mmol) Nandrolone, 0.06g (0.3mmol) [Bmim][OAc] catalyst, 10ml 1,4-dioxane, heated to 120 ° C and then reacted for 2h, after the reaction was completed, cooled to room temperature, added 30 ml of water and 20 ml of ethyl acetate were extracted, and the phases were allowed to stand. The organic phase was concentrated and crystallized to obtain the target product. The yield was 64%.
References:
CN109678718,2019,A Location in patent:Paragraph 0036
131447-69-3
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100-51-6
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1255-49-8
268 suppliers
$17.00/5mg
58-22-0
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$21.00/1mg
645-45-4
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$15.00/5g
1255-49-8
268 suppliers
$17.00/5mg