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ChemicalBook CAS DataBase List Tetrahydropyran

Tetrahydropyran synthesis

15synthesis methods
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Yield:142-68-7 270 mg

Reaction Conditions:

with hydrogen at 120; under 30003 Torr; for 48 h;

Steps:

8 Example 8

Weigh 2.0 g, weigh 2.0 mg of Cp*Ir catalyst, and its ligand structure is: the anion is OTf. The system hydrogen pressure was 4 MPa, the temperature was 120 ° C, and the reaction time was 48 hours. The final product was analyzed by gas-mass spectrometry to give a tetrahydropyran of 270 mg.

References:

CN109836402,2019,A Location in patent:Paragraph 0030-0031

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