TRIS(2-CHLOROETHYL)AMINE HYDROCHLORIDE synthesis
- Product Name:TRIS(2-CHLOROETHYL)AMINE HYDROCHLORIDE
- CAS Number:817-09-4
- Molecular formula:C6H13Cl4N
- Molecular Weight:240.99
102-71-6
758 suppliers
$18.00/100g
817-09-4
60 suppliers
$88.00/100mg
Yield:817-09-4 100%
Reaction Conditions:
with thionyl chloride in 1,2-dichloro-ethane for 4 h;Reflux;
Steps:
2
Into a 1 L flask, equipped with a refluxing condenser, is added 29.8 g (0.20 mole) of triethanolamine, 300 mL of dichloroethane, then 51.0 mL of thionyl chloride. The mixture is heated to reflux for 4 hrs. The reaction is quenched by adding 20 mL of methanol. Removal of solvent gives a white crystalline mass of tris(2-chloroethylamine) hydrochloride in quantitative yield.
References:
Hu, Songzhou US2015/299113, 2015, A1 Location in patent:Paragraph 0050
637-39-8
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$25.00/25 g
817-09-4
60 suppliers
$88.00/100mg
7719-09-7
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$15.00/10g
102-71-6
758 suppliers
$18.00/100g
817-09-4
60 suppliers
$88.00/100mg