| Identification | Back Directory | [Name]
4-PyriMidinaMine, 6-chloro-2-(2-pyridinyl)- | [CAS]
1014720-73-0 | [Synonyms]
PyriMidinaMine, 6-chloro-2-(2-pyridinyl)-
6-Chloro-2-(pyridin-2-yl)pyrimidin-4-amine
4-PyriMidinaMine, 6-chloro-2-(2-pyridinyl)-
6-chloro-2-pyridin-2-yl-pyrimidin-4-ylamine
6-chloro-2-(2-pyridin-2-yl)pyriMidin-4-ylaMine | [EINECS(EC#)]
604-604-1 | [Molecular Formula]
C9H7ClN4 | [MOL File]
1014720-73-0.mol | [Molecular Weight]
206.63 |
| Chemical Properties | Back Directory | [Boiling point ]
296.4±22.0 °C(Predicted) | [density ]
1.390±0.06 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2–8 °C | [pka]
0.77±0.10(Predicted) |
| Hazard Information | Back Directory | [Synthesis]
General procedure for the synthesis of 2-(2-pyridyl)-6-chloro-4-amino pyrimidine from 4,6-dichloro-2-(2-pyridyl)pyrimidine: 4,6-dichloro-2-(2-pyridyl)pyrimidine (210 mg, 0.93 mmol) was dissolved in ethanol (2 ml) in a microwave reaction tube. NH4OH (35% aqueous solution, 2.0 ml, 18.58 mmol) was added to this solution. The reaction mixture was heated in a microwave reactor at 100°C for 30 min. After completion of the reaction, the mixture was concentrated under vacuum. Purification was carried out by grinding the residue and washing with isopropanol to afford 2-(2-pyridyl)-6-chloro-4-aminopyrimidine (135 mg, 70% yield). | [References]
[1] Patent: US2012/202806, 2012, A1 |
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