| Identification | Back Directory | [Name]
2-bromo-6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one | [CAS]
1078150-17-0 | [Synonyms]
2-Bromo-6,7-dihydrothieno[3,2-c]pyridin-4(5H)
2-bromo-4H,5H,6H,7H-thieno[3,2-c]pyridin-4-one
2-bromo-6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one
Thieno[3,2-c]pyridin-4(5H)-one, 2-bromo-6,7-dihydro- | [Molecular Formula]
C7H6BrNOS | [MDL Number]
MFCD11656583 | [MOL File]
1078150-17-0.mol | [Molecular Weight]
232.1 |
| Chemical Properties | Back Directory | [Boiling point ]
471.8±45.0 °C(Predicted) | [density ]
1.726±0.06 g/cm3(Predicted) | [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [pka]
14.05±0.20(Predicted) | [Appearance]
Off-white to pale purple Solid |
| Hazard Information | Back Directory | [Synthesis]
Step (a) 6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one (lactam 2) was dissolved in acetic acid and bromination reaction was carried out by dropwise addition of bromine (Br2) at room temperature, and after completion of the reaction, 2-bromo-6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one (Intermediate 3) was obtained in 75% yield. | [References]
[1] Organic and Biomolecular Chemistry, 2016, vol. 14, # 27, p. 6398 - 6402
[2] Patent: WO2016/205534, 2016, A1. Location in patent: Page/Page column 24 |
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