| Identification | Back Directory | [Name]
2-AMINO-3-BROMOPHENOL | [CAS]
116435-77-9 | [Synonyms]
2-AMINO-3-BROMOPHENOL
2-Bromo-6-hydroxyaniline
Phenol, 2-amino-3-bromo-
2-Amino-3-bromophenol 97+%
2-Amino-3-bromophenol 98+%
2-Amino-3-bromophenol CAS NO.116435-77-9
High quality 2-Amino-3-bromophenol CAS NO.116435-77-9 | [Molecular Formula]
C6H6BrNO | [MDL Number]
MFCD08445676 | [MOL File]
116435-77-9.mol | [Molecular Weight]
188.02 |
| Chemical Properties | Back Directory | [Melting point ]
138℃ | [Boiling point ]
266℃ | [density ]
1.768 | [Fp ]
115℃ | [storage temp. ]
Keep in dark place,Inert atmosphere,2-8°C | [form ]
powder | [pka]
8.79±0.10(Predicted) | [color ]
Light brown | [InChI]
InChI=1S/C6H6BrNO/c7-4-2-1-3-5(9)6(4)8/h1-3,9H,8H2 | [InChIKey]
JBNSVEGZVHJLMS-UHFFFAOYSA-N | [SMILES]
C1(O)=CC=CC(Br)=C1N |
| Hazard Information | Back Directory | [Uses]
2-Amino-3-bromophenol is a useful reagent for organic synthesis and other chemical processes. | [Synthesis]
Step B: Synthesis of 2-amino-3-bromophenol. A dichloromethane solution (10 mL, 10 mmol) of 1.0 M boron tribromide was added slowly and dropwise via syringe to a dichloromethane (30 mL) solution of 6-bromo-2-methoxyaniline (1.01 g, 5 mmol) under cooling conditions in an ice bath. The reaction mixture was slowly warmed to room temperature and stirred continuously overnight. Upon completion of the reaction, the reaction was quenched by the addition of methanol (10 mL) and the solvent was subsequently removed by rotary evaporator to afford the target product 2-amino-3-bromophenol (0.87 g, 92% yield). | [References]
[1] Patent: US6291511, 2001, B1 |
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