| Identification | Back Directory | [Name]
3-Methyl-1H-pyrazolo[3,4-b]pyridine-5-amine | [CAS]
1186608-73-0 | [Synonyms]
5-Amino-3-iodo-1H-pyrazolo[3,4-b]pyridine
3-Methyl-1H-pyrazolo[3,4-b]pyridin-5-aMine
5-AMino-3-Methyl-1H-pyrazolo[3,4-b]pyridine
3-Methyl-1H-pyrazolo[3,4-b]pyridine-5-amine
1H-Pyrazolo[3,4-b]pyridin-5-amine, 3-methyl- | [Molecular Formula]
C7H8N4 | [MDL Number]
MFCD13193614 | [MOL File]
1186608-73-0.mol | [Molecular Weight]
148.17 |
| Hazard Information | Back Directory | [Synthesis]
GENERAL STEPS: 3-methyl-5-nitro-1H-pyrazolo[3,4-b]pyridine (39 mg, 0.22 mmol) and 10% Pd/C (12 mg, 0.011 mmol) were added to a 25 mL round bottom flask. Ethanol (10 mL) was then added and hydrogen was passed into the reaction mixture for 15 min. The reaction flask was stirred under a hydrogen balloon for 4 h. After completion of the reaction, it was filtered through a 0.45 μm PVDF filter. Finally, the solvent was removed to afford 3-methyl-1H-pyrazolo[3,4-b]pyridin-5-amine solid (30 mg, 92% yield). | [References]
[1] Patent: WO2009/111279, 2009, A1. Location in patent: Page/Page column 84
[2] Patent: WO2012/135631, 2012, A1. Location in patent: Page/Page column 17
[3] Patent: WO2005/9958, 2005, A1. Location in patent: Page 180-181 |
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