| Identification | Back Directory | [Name]
BENZENETHIOSULFONIC ACID S-PHENYL ESTER | [CAS]
1212-08-4 | [Synonyms]
NSC74657
Phenylphenylthiosulfone
Phenylbenzenethiosulfonate
S- phenylthiophenylsulfone
S-PHENYL BENZENETHIOSULFATE
(phenylthio)sulfonylbenzene
phenylsulfanylsulfonylbenzene
S-PHENYL BENZENETHIOSULFONATE
S-phenylbenzenethiosulphonate
S-PHENYLBENZENESULFONOTHIOATE
(Phenylsulfonyl)phenyl sulfide
Phenyl(phenylsulfonyl) sulfide
benzenesulfonylsulfanylbenzene
S-Phenylbenzenemonothiosulfonate
Benzenethiosulfonic acid S-phenyl
S-Phenyl benzenethiosulfonate 99%
BENZENETHIOSULFONIC ACID S-PHENYL ESTER
Benzenesulfonicacid,thio-,S-phenylester
Benzenesulfonothioic acid, S-phenyl ester
TIANFUCHEM 1212-08-4 BENZENETHIOSULFONIC ACID S-PHENYL ESTER | [EINECS(EC#)]
214-919-1 | [Molecular Formula]
C12H10O2S2 | [MDL Number]
MFCD00014738 | [MOL File]
1212-08-4.mol | [Molecular Weight]
250.34 |
| Hazard Information | Back Directory | [Uses]
S-Phenyl Benzenethiosulfonate is an high potency antifungal thiosulfonate that were tested against Aspergillus niger and Aspergillus flavus. | [Preparation]
BENZENETHIOSULFONIC ACID S-PHENYL ESTER can be prepared by oxidation of Diphenyl Disulfide with 30% Hydrogen Peroxide (72%). | [Synthesis Reference(s)]
Journal of the American Chemical Society, 99, p. 4405, 1977 DOI: 10.1021/ja00455a032
Tetrahedron Letters, 10, p. 1239, 1969 | [Purification Methods]
Recrystallise the disulfoxide from EtOH or MeOH. It has also been purified from phenylsulfide impurities by dissolving in CHCl3, washing with aqueous saturated NaHCO3, drying (Na2SO4), filtering, evaporating the filtrate, and the residual oil is passed through a silica gel column (600g) and eluted with hexane/*C6H6 (1L, 4:1, eluting PhSSPh) then *C6H6 (1L) which elutes PhSSO2Ph. [Trost & Massiot J Am Chem Soc 99 4405 1977, Knoevenagel & R.mer Chem Ber 56 215 1923, Beilstein 11 IV 220.] |
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J & K SCIENTIFIC LTD.
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https://www.jkchemical.com |
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Energy Chemical
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400-0056266 |
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www.energy-chemical.com |
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Sigma-Aldrich
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https://www.sigmaaldrich.cn |
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