| Identification | Back Directory | [Name]
Methyl 4-aMino-2-Methyl-5-nitrobenzoate | [CAS]
1260848-51-8 | [Synonyms]
Methyl 4-aMino-2-Methyl-5-nitrobenzoate
Benzoic acid, 4-amino-2-methyl-5-nitro-, methyl ester | [Molecular Formula]
C9H10N2O4 | [MDL Number]
MFCD08458965 | [MOL File]
1260848-51-8.mol | [Molecular Weight]
210.19 |
| Chemical Properties | Back Directory | [Boiling point ]
403.7±40.0 °C(Predicted) | [density ]
1.332±0.06 g/cm3(Predicted) | [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [pka]
-2.34±0.25(Predicted) |
| Hazard Information | Back Directory | [Synthesis]
Step 3. Ammonia (g) was passed into a solution of THF (180 mL) containing methyl 4-fluoro-2-methyl-5-nitrobenzoate (30 g, 140.74 mmol) and the reaction was carried out for 5 hours at room temperature. Upon completion of the reaction, the reaction was quenched with water (500 mL). The solid was collected by filtration to afford methyl 4-amino-2-methyl-5-nitrobenzoate as a yellow solid (24.5 g, 83% yield).LC/MS (ES, m/z): [M+H]+ 211.0.1H-NMR (300 MHz, CDCl3): δ8.85(s, 1H), 6.64(s, 1H), 3.88(s, 3H) , 2.61(s, 3H). | [References]
[1] Patent: US2012/277224, 2012, A1. Location in patent: Page/Page column 61 |
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Cool Pharm, Ltd
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021-60455363 18019463053 |
| Website: |
www.coolpharm.com |
| Company Name: |
Energy Chemical
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| Tel: |
021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
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