| Identification | Back Directory | [Name]
2-(7-METHOXYNAPHTHALEN-1-YL)ETHANAMINE | [CAS]
138113-09-4 | [Synonyms]
Agomelatine intermediate
7-Methoxy-1-Napthtaleneethanamine
7-Methoxy-1-naphthaleneethanaMine
2-(7-Methoxynaphth-1-yl)ethylamine
2-(7-METHOXYPHTHALEN-1-YL)ETHAMINE
2-(7-Methoxy-1-naphthyl)ethanamine
2-(7-Methoxynaphthalen-1-yl)ethylaMine
2-(7-METHOXYNAPHTHALEN-1-YL)ETHANAMINE
2-(7-methoxynaphthalen-1-yl)ethan-1-amine
(3-oxo-1lambda3,2-benziodoxol-2-yl)acetate
2-(7-Methoxynaphthalen-1-yl)ethanamine(N-1)
2-(7-methoxy naphthalen-1-yl)ethanamine ( 138113-09-4) | [EINECS(EC#)]
604-062-5 | [Molecular Formula]
C13H15NO | [MDL Number]
MFCD09744147 | [MOL File]
138113-09-4.mol | [Molecular Weight]
201.26 |
| Questions And Answer | Back Directory | [Preparation]
21.5 g (0.1 mol) of (7-methoxy-1-naphthyl)acetamide was dissolved in 160 mL of toluene at room temperature. 26.9 g (0.2 mol) of TMDS and 28.4 g (0.1 mol) of Ti(OiPr)4 were added with stirring. The mixture was heated to 100°C and stirred overnight. TLC showed that the starting material had disappeared, and the main product, 7-methoxy-1-naphthylethylamine, was formed. After cooling to room temperature, HCl gas was introduced, and the product precipitated as a hydrochloride salt. Filtering and drying yielded 20.3 g of 2-(7-METHOXYNAPHTHALEN-1-YL)ETHANAMINE hydrochloride with a chemical purity exceeding 99% and a yield of 85.4%. |
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