ChemicalBook--->CAS DataBase List--->1431-39-6

1431-39-6

1431-39-6 Structure

1431-39-6 Structure
IdentificationBack Directory
[Name]

DANSYLAMIDE
[CAS]

1431-39-6
[Synonyms]

DNSA
DANSYLAMIDE
Dansylamide,99%
DansylaMide, 99% 1GR
Dansyl amide, DNSA
Dansylamide [for Fluorometry]
5-DIMETHYLAMINONAPHTHALENE-1-SULFONAMIDE
5-DIMETHYLAMINO-1-NAPHTHALENESULFONAMIDE
5-(dimethylamino)naphthalene-1-sulphonamide
5-(DiMethylaMino)-1-naphthalenesulfonaMide 99%
5-Dimethylamino-1-naphthalenesulphonamide~DNSA
[EINECS(EC#)]

215-854-1
[Molecular Formula]

C12H14N2O2S
[MDL Number]

MFCD00004000
[MOL File]

1431-39-6.mol
[Molecular Weight]

250.32
Chemical PropertiesBack Directory
[Appearance]

white to light yellow fine crystalline powder
[Melting point ]

218-221 °C(lit.)
[Boiling point ]

435.4±37.0 °C(Predicted)
[density ]

1.2391 (rough estimate)
[refractive index ]

1.5950 (estimate)
[storage temp. ]

−20°C
[solubility ]

soluble in Dimethylformamide
[form ]

Fine Crystalline Powder
[pka]

10.29±0.30(Predicted)
[color ]

White to light yellow
[BRN ]

2217203
[InChI]

InChI=1S/C12H14N2O2S/c1-14(2)11-7-3-6-10-9(11)5-4-8-12(10)17(13,15)16/h3-8H,1-2H3,(H2,13,15,16)
[InChIKey]

TYNBFJJKZPTRKS-UHFFFAOYSA-N
[SMILES]

C1(S(N)(=O)=O)=C2C(C(N(C)C)=CC=C2)=CC=C1
[CAS DataBase Reference]

1431-39-6
Hazard InformationBack Directory
[Chemical Properties]

white to light yellow fine crystalline powder
[Uses]

5-(Dimethylamino)-1-naphthalenesulfonamide (DNSA) was used as starting reagent in the synthesis of 2,6-disubstituted pyridines, 6-substituted 2,2′-bipyridines and 6,6′-disubstituted 2,2′-bipyridines. It was also used as fluorescent probe in the determination of concentration of human carbonic anhydrase II-DNSA in solutions.
[Synthesis]

Synthesis and characterization of dansylamide (DNS-NH2): a solution of sodium sulfide (43 mg, 0.18 mmol) in 0.4 mL H2O was added to a stirred 2 mL solution of dansyl chloride in 17 mL acetonitrile. The reaction mixture was stirred at room temperature for
Safety DataBack Directory
[Safety Statements ]

22-24/25
[WGK Germany ]

3
[HS Code ]

29350090
[Storage Class]

11 - Combustible Solids
Spectrum DetailBack Directory
[Spectrum Detail]

DANSYLAMIDE(1431-39-6)MS
DANSYLAMIDE(1431-39-6)1HNMR
DANSYLAMIDE(1431-39-6)13CNMR
DANSYLAMIDE(1431-39-6)IR1
DANSYLAMIDE(1431-39-6)IR2
DANSYLAMIDE(1431-39-6)Raman
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