15430-62-3

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15430-62-3 Structure

Identification	Back Directory
[Name] 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE
[CAS] 15430-62-3
[Synonyms] Einecs 239-441-0 Bromocyanodimethylacetamide 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE N,N-DIMETHYL-2-BROMO-2-CYANOACETAMIDE 2-bromo-2-cyano-n,n-dimethyl-acetamid Acetamide, 2-bromo-2-cyano-N,N-dimethyl- 2-BROMO-2-CYANO-N N-DIMETHYLACETAMIDE 90+% 2-(N,N-DIMETHYLCARBAMOYL)-2-BROMOACETONITRILE 2-Bromo-2-cyano-N,N-dimethylacetamide N,N-Dimethyl-2-bromo-2-cyanoacetamide 2-(N,N-Dimethylcarbamoyl)-2-bromoacetonitrile
[EINECS(EC#)] 239-441-0
[Molecular Formula] C5H7BrN2O
[MDL Number] MFCD00040509
[MOL File] 15430-62-3.mol
[Molecular Weight] 191.03

Chemical Properties	Back Directory
[Melting point ] 57°C
[Boiling point ] 135 °C / 3mmHg
[density ] 1.560±0.06 g/cm3(Predicted)
[solubility ] sol ethanol, benzene, chloroform, ethyl acetate, and THF; insol petroleum ether and hexane; slightly sol hot ether, isopropyl alcohol, and H2O
[pka] -0.65±0.70(Predicted)
[EPA Substance Registry System] Acetamide, 2-bromo-2-cyano-N,N-dimethyl- (15430-62-3)

Safety Data	Back Directory
[Symbol(GHS) ] GHS07
[Signal word ] Warning
[Hazard statements ] H302+H312+H332-H315-H319
[Precautionary statements ] P261-P264-P270-P271-P280-P301+P312+P330-P302+P352+P312+P362+P364-P304+P340+P312-P305+P351+P338+P337+P313-P501
[Hazard Codes ] Xn
[Risk Statements ] 36/37/38-36-22
[Safety Statements ] 26-36/37/39
[TSCA ] TSCA listed
[HS Code ] 2926907090

Hazard Information	Back Directory
[Uses] 2-Bromo-2-cyano-n,n-dimethylacetamide is a monobrominating agent that is selective for the α-carbon of enolizable ketones.
[Preparation] Via bromination of 2-cyano-N,N-dimethylacetamide with Br2 in AcOH/Ac2O at 8- 10 °C.
[storage] The reagent is fairly stable at rt. For long storage, keep at 0-10 °C, shielded from light. This reagent should be handled in a fume hood.

Spectrum Detail	Back Directory
[Spectrum Detail] 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE(15430-62-3)MS 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE(15430-62-3)¹HNMR 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE(15430-62-3)¹³CNMR 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE(15430-62-3)IR1 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE(15430-62-3)IR2

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