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329944-59-4

329944-59-4 Structure

329944-59-4 Structure
IdentificationBack Directory
[Name]

(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE
[CAS]

329944-59-4
[Synonyms]

Methanone, (3-bromo-5-chlorophenyl)(5-chloro-2-methoxyphenyl)-
(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE
[Molecular Formula]

C14H9BrCl2O2
[MDL Number]

MFCD09031573
[MOL File]

329944-59-4.mol
[Molecular Weight]

360.03
Chemical PropertiesBack Directory
[Boiling point ]

479.3±45.0 °C(Predicted)
[density ]

1.554±0.06 g/cm3(Predicted)
Hazard InformationBack Directory
[Preparation]

A solution of 1,3-dibromo-5-chlorobenzene (1 mmol) in ethyl ether was cooled to ?78° and n-butyllithium in hexane (1.1 mmol) was added over 2 min.The reaction mixture was stirred at ?78° for an additional 10 min, and then 5-chloro-N,2-dimethoxy-N-methylbenzamide (1 mmol) was added in small portions over 4 min. The reaction mixture was stirred at ?78° for 1.25 h and then allowed to warm to r.t. and stirred for 14 h (97%).
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