| Identification | Back Directory | [Name]
4,4'-OXYBISBENZOYL CHLORIDE | [CAS]
7158-32-9 | [Synonyms]
ODBC
BPDC
4.4-oxybisbenzoic chloride
4,4'-OXYBISBENZOYL CHLORIDE
4,4-OXY-DI-BENZOYLCHLORIDE
p,p'-Oxybis(benzoyl chloride)
Benzoyl chloride, 4,4'-oxybis-
4-(Chlorocarbonyl)phenyl ether
4,4'-Oxybis(benzoylChloride)>
Bis(4-chlorocarbonylphenyl) Ether
4.4-oxybisbenzoic chloride (DEDC)
4,4'-bis(chlorocarbonyl)diphenyl oxide
4,4'-Bis(chlorocarbonyl)diphenyl Ether
4,4'-Oxybisbenzoyl chloride(DEDC/ODBC)
Diphenyl oxide 4,4'-dicarbonyl chloride
Diphenyl ether 4,4'-dicarbonyl dichloride
4,4'-OXYBISBENZOYL CHLORIDE in stock Factory
4-(4-carbonochloridoylphenoxy)benzoyl chloride
4,4-Dicarboxylic acid diphenyl oxide dichloroanhydride | [EINECS(EC#)]
808-159-5 | [Molecular Formula]
C14H8Cl2O3 | [MDL Number]
MFCD00496619 | [MOL File]
7158-32-9.mol | [Molecular Weight]
295.12 |
| Chemical Properties | Back Directory | [Melting point ]
22-23℃ | [Boiling point ]
404℃ | [density ]
1.386 | [Fp ]
164℃ | [storage temp. ]
Inert atmosphere,2-8°C | [solubility ]
soluble in Toluene | [form ]
powder to crystaline | [color ]
White to Almost white | [InChI]
InChI=1S/C14H8Cl2O3/c15-13(17)9-1-5-11(6-2-9)19-12-7-3-10(4-8-12)14(16)18/h1-8H | [InChIKey]
OSUWBBMPVXVSOA-UHFFFAOYSA-N | [SMILES]
O(C1=CC=C(C=C1)C(Cl)=O)C1=CC=C(C=C1)C(Cl)=O |
| Hazard Information | Back Directory | [Uses]
4,4'-OXYBISBENZOYL CHLORIDE is a useful research chemical. | [Synthesis]
4,4′-oxybisbenzaldehyde is reacted with chlorine to produce 4,4'-Oxybis(benzoyl Chloride) in high yield without using a large amount of reaction solvent. A 300 ml four-necked flask equipped with a stirrer, a thermometer and a reflux condenser was charged with 90.6 g (0.40 mol) of 4,4′-oxybisbenzaldehyde and 158.6 g of PCBTF, and heated and stirred to 143 ° C. The temperature was raised to. A high pressure mercury lamp was turned on and irradiated with light. The reaction was started by supplying chlorine gas at a chlorine gas blowing rate of 0.06 mol / hour so as to maintain a reaction temperature of 143 ° C. (reflux). After 15 hours from the start of the reaction, disappearance of the raw materials was confirmed by gas chromatography, and the reaction was completed. When this was analyzed using gas chromatography, the reaction yield of 4,4'-Oxybis(benzoyl Chloride) was 98.6% by mass. | [References]
[1] Patent: JP2017/149660, 2017, A. Location in patent: Paragraph 0232; 0233
[2] Patent: JP2017/149650, 2017, A. Location in patent: Paragraph 0188-0189
[3] Patent: JP2017/141213, 2017, A. Location in patent: Paragraph 0117
[4] Patent: JP2017/141212, 2017, A. Location in patent: Paragraph 0186
[5] Patent: JP2017/141211, 2017, A. Location in patent: Paragraph 0148 |
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| Company Name: |
J & K SCIENTIFIC LTD.
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| Telephone: |
18210857532 18210857532 |
| Website: |
https://www.jkchemical.com |
| Company Name: |
Energy Chemical
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| Telephone: |
400-0056266 |
| Website: |
www.energy-chemical.com |
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