| Identification | Back Directory | [Name]
6-broMo-N-Methyl-1,3-benzothiazol-2-aMine | [CAS]
75104-92-6 | [Synonyms]
2-Benzothiazolamine, 6-bromo-N-methyl-
6-BroMo-N-Methylbenzo[d]thiazol-2-aMine
(6-Bromo-benzothiazol-2-yl)-methyl-amine
6-broMo-N-Methyl-1,3-benzothiazol-2-aMine | [Molecular Formula]
C8H7BrN2S | [MDL Number]
MFCD13190227 | [MOL File]
75104-92-6.mol | [Molecular Weight]
243.12 |
| Chemical Properties | Back Directory | [Melting point ]
227-228 °C | [Boiling point ]
328.461±34.00 °C(Press: 760.00 Torr)(predicted) | [density ]
1.713±0.06 g/cm3(Temp: 25 °C; Press: 760 Torr)(predicted) | [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [pka]
3.484±0.10(predicted) | [Appearance]
White to off-white Solid |
| Hazard Information | Back Directory | [Synthesis]
In a sealed reaction tube, 6-bromo-2-chlorobenzo[d]thiazole (701) (0.5 g, 2.0 mmol) was dissolved in methylamine solution (20 mL), and the resulting mixture was stirred and reacted at 60 °C overnight. Upon completion of the reaction, the mixture was cooled to room temperature, concentrated under reduced pressure to remove the solvent and quenched by the addition of water (20 mL). The precipitated solid was collected by filtration to afford the target product 6-bromo-N-methylbenzo[d]thiazol-2-amine (702) (0.43 g, 87.9% yield). The product was analyzed by ESI-MS and showed (M + H)+ m/z: 242.8. | [References]
[1] Patent: US2015/225407, 2015, A1. Location in patent: Paragraph 0416
[2] Recueil des Travaux Chimiques des Pays-Bas, 1934, vol. 53, p. 1
[3] Patent: WO2017/46739, 2017, A1. Location in patent: Page/Page column 50 |
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| Company Name: |
Energy Chemical
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| Telephone: |
021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
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