| Identification | Back Directory | [Name]
4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID | [CAS]
91652-00-5 | [Synonyms]
4-((6-(methacryloyloxy)hexyl)oxy)benzoic acid
4-[6-(2-METHYL-ACRYLOXY)-HEXYLOXY]-BENZOIC ACID
4-(6-METHACRYLOYLOXY-N-HEX-1-YLOXY)BENZOIC ACID
4-[6-(2-METHYL-ACRYLOYLOXY)HEXYLOXY]BENZOIC ACID
4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID
4-[[6-[(2-methyl-1-oxo-2-propen-1-yl)oxy]hexyl]oxy]Benzoic acid
Benzoic acid, 4-[[6-[(2-methyl-1-oxo-2-propen-1-yl)oxy]hexyl]oxy]- | [Molecular Formula]
C17H22O5 | [MDL Number]
MFCD01166369 | [MOL File]
91652-00-5.mol | [Molecular Weight]
306.35 |
| Chemical Properties | Back Directory | [Melting point ]
75-79 °C(Solv: isopropanol (67-63-0)) | [Boiling point ]
457.9±25.0 °C(Predicted) | [density ]
1.122±0.06 g/cm3(Predicted) | [pka]
4.48±0.10(Predicted) |
| Hazard Information | Back Directory | [Uses]
4-{[6-(Methacryloyloxy)hexyl]oxy}benzenecarboxylic acid is a useful research chemical compound. | [Preparation]
The preparation of 4-([6-(methacryloyloxy)hexyl]oxy)benzenecarboxylic acid is as follows:6-(4-Formylphenoxy)hexyl methacrylate in an amount of 116.14 g, 2100 mL of methanol, an aqueous sodium dihydrogen phosphate solution (obtained by dissolving 43 g of sodium dihydrogen phosphate dihydrate in 570 mL of water) and 73 mL of a 30% hydrogen peroxide solution were added one by one. An aqueous sodium chlorite solution (obtained by dissolving 61.9 g of sodium chlorite with the purity of 80% in 500 mL of water) was added by dropping. After dropping, the reaction liquid was stirred at 45° C. for 3 hours, and the reaction was finished. After slowly cooling the reaction liquid to 20° C., 2250 mL of water was dropped to the reaction liquid, and a solid was precipitated. The solid was collected by filtration, and 72.7 g of 4-((6-(methacryloyloxy)hexyl)oxy)benzoic acid was thus obtained.
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