| Identification | Back Directory | [Name]
Phenol, 4-bromo-3-ethyl- | [CAS]
99873-30-0 | [Synonyms]
3-ethyl-4-broMophenol
4-broMo-3-ethylphenol
Phenol, 4-bromo-3-ethyl- | [Molecular Formula]
C8H9BrO | [MDL Number]
MFCD16997652 | [MOL File]
99873-30-0.mol | [Molecular Weight]
201.06 |
| Chemical Properties | Back Directory | [Boiling point ]
267.0±20.0 °C(Predicted) | [density ]
1.469±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [pka]
9.49±0.18(Predicted) | [Appearance]
White to off-white Solid |
| Hazard Information | Back Directory | [Synthesis]
Under ice bath cooling at 0°C, 7.33 g of 3-ethylphenol was dissolved in 600 mL of chloroform, followed by the addition of 10.7 g of N-bromosuccinimide. The reaction mixture was gradually warmed to room temperature and stirred continuously for 2 hours. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure. The resulting crude product was purified by silica gel column chromatography to give 7.25 g of 4-bromo-3-ethylphenol (named 45A). | [References]
[1] Patent: WO2011/34828, 2011, A1. Location in patent: Page/Page column 84
[2] Patent: EP2177513, 2010, A1. Location in patent: Page/Page column 28
[3] Patent: CN105392779, 2016, A. Location in patent: Paragraph 1351; 1352; 1353; 1354
[4] Patent: US2016/159755, 2016, A1. Location in patent: Paragraph 0707; 0708 |
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| Company Name: |
Beijing Kemik-Chem Co. Ltd.
|
| Tel: |
010-56130310 15313443500 |
| Website: |
www.chemicalbook.com/ShowSupplierProductsList30424/0_EN.htm |
| Company Name: |
Energy Chemical
|
| Tel: |
021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
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