Benzyl4-iodobenzoate
- CAS No.
- 136618-42-3
- Chemical Name:
- Benzyl4-iodobenzoate
- Synonyms
- Benzyl4-iodobenzoate;Benzoic acid, 4-iodo-, phenylmethyl ester
- CBNumber:
- CB02499132
- Molecular Formula:
- C14H11IO2
- Molecular Weight:
- 338.14
- MDL Number:
- MFCD18072656
- MOL File:
- 136618-42-3.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302 |
| Precautionary statements | P280-P305+P351+P338 |
Benzyl4-iodobenzoate price More Price(38)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS34031 | Benzyl 4-iodobenzoate 95% | 136618-42-3 | 1g | $88 | 2026-06-04 | Buy |
| Activate Scientific | AS34031 | Benzyl 4-iodobenzoate 95% | 136618-42-3 | 5g | $181 | 2026-06-04 | Buy |
| Matrix Scientific | 074737 | Benzyl 4-iodobenzoate | 136618-42-3 | 1.00g | $347 | 2026-05-18 | Buy |
| Matrix Scientific | 074737 | Benzyl 4-iodobenzoate | 136618-42-3 | 5.00g | $899 | 2026-05-18 | Buy |
| Matrix Scientific | 074737 | Benzyl 4-iodobenzoate | 136618-42-3 | 10.00g | $1286 | 2026-05-18 | Buy |
Benzyl4-iodobenzoate Chemical Properties,Uses,Production
Synthesis
619-58-9
100-39-0
136618-42-3
General procedure: 4-Iodobenzoic acid (15.62 g, 63 mmol, 1.05 eq.) was suspended in anhydrous DMF (90 mL, 6 vol.) under nitrogen protection, potassium carbonate (8.7 g, 63 mmol, 1.05 eq.) was added, and stirred for 10 minutes. Subsequently, benzyl bromide (10.25 g, 7.13 mL, 60 mmol, 1 eq.) was slowly added dropwise for a controlled time of about 5 minutes. The reaction mixture was continued to be stirred at room temperature for 6.25 hours. Upon completion of the reaction, the mixture was transferred to a partition funnel and extracted with ether (200 mL) and water (200 mL) by partition. The aqueous phase was extracted once more with ether, and the organic phases were combined and washed sequentially with water, aqueous lithium chloride and brine. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to afford benzyl 4-iodobenzoate (18.38 g, 86% yield) as a white crystalline solid. The product was analyzed by LCMS: tRET = 3.81 min, 70% ES + ve 376,356 (artifactual peak appeared at 1.48 min, 28%).1H NMR (400 MHz, DMSO-d6) δ ppm: 7.92 (d, 2H), 7.74 (d, 2H), 7.46 (d, 2H), 7.35-7.42 (m, 3H ), 5.34 (s, 2H).
References
[1] Patent: WO2009/74590, 2009, A1. Location in patent: Page/Page column 59-60
[2] Patent: WO2009/50220, 2009, A1. Location in patent: Page/Page column 42
Benzyl4-iodobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Benzyl4-iodobenzoate Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| 9ding chemical ( Shanghai) Limited | 4009209199 | sales@9dingchem.com | China | 18201 | 56 |
| SynAsst Chemical. | 021-60343070 | China | 12731 | 55 | |
| Shanghai HuanChuan Industry Co.,Ltd. | 021-61478794 | sales@hcshhai.com | China | 9781 | 50 |
| Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd | 18210788515; 18210788515 | zhuzixin999@163.c0m | China | 4999 | 55 |
| Quzhou AMK BioTech Co., Ltd | 0570-3081766 18357083060 | sales@qzamkbio.com | China | 1199 | 55 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Hangzhou Molcore Biopharmatech Co.,Ltd | 400-711-5280 86-571-81025280 | sales@molcore.com | China | 9957 | 58 |
| Aikon International Limited | 025-66061636 19370895928 | qqyang@aikonchem.com | China | 15810 | 58 |
| Suzhou Nuoouman Biological Technology Co., Ltd. | 15026866316 | 180642609@qq.com | China | 4969 | 58 |
