2-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol
- CAS No.
- 651030-56-7
- Chemical Name:
- 2-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol
- Synonyms
- 2-(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl);(3-(2-hydroxyethyl)phenyl)boronic acid pinacol ester;2-[3-(TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL]ETHANOL;3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzeneethanol;Benzeneethanol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;2-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol;2-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethan-1-ol
- CBNumber:
- CB02554154
- Molecular Formula:
- C14H21BO3
- Molecular Weight:
- 248.13
- MDL Number:
- MFCD18733920
- MOL File:
- 651030-56-7.mol
- MSDS File:
- SDS
2-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol price More Price(47)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Biosynth | BBB03056 | 2-(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethan-1-ol | 651030-56-7 | 5g | $500 | 2026-06-04 | Buy |
| AK Scientific | AMTB1313 | 2-(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethan-1-ol 97% | 651030-56-7 | 100mg | $108 | 2026-06-04 | Buy |
| AK Scientific | AMTB1313 | 2-(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethan-1-ol 97% | 651030-56-7 | 250mg | $190 | 2026-06-04 | Buy |
| AK Scientific | AMTB1313 | 2-(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethan-1-ol 97% | 651030-56-7 | 1g | $454 | 2026-06-04 | Buy |
| AK Scientific | AMTB1313 | 2-(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethan-1-ol 97% | 651030-56-7 | 5g | $1380 | 2026-06-04 | Buy |
2-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol Chemical Properties, Uses, Production
Synthesis
28229-69-8
73183-34-3
651030-56-7
Stage 1: 3-bromophenethyl alcohol (3.0 g, 15 mmol), KOAc (4.39 g, 45 mmol), bis(pinacolato)diboron (5.68 g, 22 mmol), and PdCl2(dppf)2 (0.61 g, 0.74 mmol) were dissolved in anhydrous DMSO (30 mL). The reaction mixture was heated and stirred at 120 °C for 18 h under nitrogen protection. After the reaction was completed, it was cooled to room temperature and diluted by adding EtOAc (60 mL). The reaction mixture was filtered through Celite and the filter cake was washed with EtOAc (500 mL). The combined organic phases were washed sequentially with saturated NaHCO3 solution (150 mL), water (150 mL) and brine (150 mL), dried over MgSO4, filtered and concentrated under reduced pressure. The crude product was purified by automated column chromatography using EtOAc/heptane (gradient 0-100%) as eluent, and further purified by column chromatography (33% EtOAc/heptane) to afford 2-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol as a light yellow oil (3.30 g, 89% yield).1H NMR (300 MHz, CDCl3) δ (ppm): 7.70 (2H, m), 7.35 (2H, m), 3.89 (2H, t, J = 6.6 Hz), 2.90 (2H, t, J = 6.6 Hz), 1.51 (1H, s), 1.37 (12H, s).
References
[1] Patent: WO2014/1802, 2014, A1. Location in patent: Page/Page column 41; 42
2-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanol Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai Topbiochem Technology Co., Ltd | 021-58170097 | info@topbiochem.com | China | 9510 | 58 |
| Shanghai ShiXian Chemical Technology Co., Ltd. | 13764359345 | 990877971@qq.com | China | 1917 | 50 |
| Shanghai Balmxy Pharmaceutical Co., Ltd | 021-24206007 13764915196 | sales@balmxy.com | China | 6959 | 55 |
| Suzhou Chenke Biotech Co., Ltd. | 18662408853 | 2120408911@qq.com | China | 980 | 55 |
| SuZhou ShiYa Biopharmaceuticals, Inc. | 0512-0512-52358471 17715136450 | sales@shiyabiopharm.com | China | 9814 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Amatek Scientific Co. Ltd. | 0512-56316828 400-867-5858;400-867-5858 | info@amateksci.com | China | 28760 | 58 |
| Capot Chemical Co.,Ltd. | +86-（0）57185586718 +86-13336195806 | sales@capot.com | China | 29626 | 60 |
| Aikon International Limited | 025-58851090 13913916777 | sales01@aikonchem.com | China | 15947 | 58 |
| Henan Alfachem Co.,Ltd. | 0371-55051623 18137891487 | 3983243027@qq.com | China | 9971 | 58 |
