Methyl 2-Methyl-1H-indole-6-carboxylate
- CAS No.
- 184150-96-7
- Chemical Name:
- Methyl 2-Methyl-1H-indole-6-carboxylate
- Synonyms
- @16258433383727256;Methyl 2-methyl-indole-6-carboxylate;Methyl 2-Methyl-1H-indole-6-carboxylate;2-Methyl-1H-indole-6-Carbocylic acid methyl ester;2-Methyl-1H-indole-6-carboxylic acid Methyl ester;1H-Indole-6-carboxylic acid, 2-methyl-, methyl ester
- CBNumber:
- CB02644130
- Molecular Formula:
- C11H11NO2
- Molecular Weight:
- 189.21
- MDL Number:
- MOL File:
- 184150-96-7.mol
- MSDS File:
- SDS
Methyl 2-Methyl-1H-indole-6-carboxylate price More Price(21)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Matrix Scientific | 305309 | Methyl 2-methyl-1H-indole-6-carboxylate | 184150-96-7 | 250.00mg | $63 | 2026-05-19 | Buy |
| Matrix Scientific | 305309 | Methyl 2-methyl-1H-indole-6-carboxylate | 184150-96-7 | 1.00g | $237 | 2026-05-19 | Buy |
| Matrix Scientific | 305309 | Methyl 2-methyl-1H-indole-6-carboxylate | 184150-96-7 | 5.00g | $696 | 2026-05-19 | Buy |
| Synthonix | M21978 | Methyl 2-methyl-1H-indole-6-carboxylate 97% | 184150-96-7 | 100mg | $44 | 2026-05-06 | Buy |
| Synthonix | M21978 | Methyl 2-methyl-1H-indole-6-carboxylate 97% | 184150-96-7 | 250mg | $70 | 2026-05-06 | Buy |
Methyl 2-Methyl-1H-indole-6-carboxylate Chemical Properties, Uses, Production
Synthesis
4518-10-9
67-64-1
184150-96-7
A degassing mixture was prepared from methyl 3-aminobenzoate (10.0 g, 0.061 mol) and copper(II) acetate decahydrate (36.2 g, 0.182 mol) in dimethyl sulfoxide (50 mL). Acetone (100 mL) was added to the reaction flask followed by palladium(II) acetate (0.270 g, 0.001 mol). The reaction mixture was heated at 80 °C for 48 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was filtered through a diatomaceous earth pad and the filtrate was diluted with water (80 mL). The aqueous phase was extracted with ethyl acetate (3 x 100 mL), the organic phases were combined and dried over anhydrous sodium sulfate. The organic layer was concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography using gradient elution with 5-7% ethyl acetate in hexane solution to obtain the target product methyl 2-methyl-1H-indole-6-carboxylate (LVII, 4.8 g, 83% yield) as a light yellow solid. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3) and mass spectrometry (ESI, positive mode): 1H NMR δ 8.26 (brs, 1H), 8.04 (s, 1H), 7.77 (dd, J = 8.3, 3.4 Hz, 1H), 7.50 (d, J = 8.3 Hz, 1H), 6.26 (s, 1H), 3.92 (s, 3H), 2.47 (s, 3H); MS m/z 190 (MH+).
References
[1] Patent: WO2015/73528, 2015, A1. Location in patent: Page/Page column 148-149
Methyl 2-Methyl-1H-indole-6-carboxylate Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
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