9-(3-Bromophenyl)-9-phenyl-9H-fluorene
- CAS No.
- 1257251-75-4
- Chemical Name:
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
- Synonyms
- 3-BPF;9-(3-Bromophenyl)-9-phenyl-fluorene;9-(3-bromophenyl)-9-phenyl-9H-fluoren;9-(3-Bromophenyl)-9-phenyl-9H-fluorene;9H-Fluorene, 9-(3-bromophenyl)-9-phenyl-;9-(3-bromophenyl-D4)-9-phenyl-9H-fluorene;9-(3-Bromophenyl)-9-phenyl-9H-fluorene ISO 9001：2015 REACH
- CBNumber:
- CB13044385
- Molecular Formula:
- C25H17Br
- Molecular Weight:
- 397.31
- MDL Number:
- MFCD30187277
- MOL File:
- 1257251-75-4.mol
- MSDS File:
- SDS
| Melting point | 131.0 to 135.0 °C |
|---|---|
| Boiling point | 480.5±24.0 °C(Predicted) |
| Density | 1.363±0.06 g/cm3(Predicted) |
| storage temp. | Storage temp. 2-8°C |
| solubility | soluble in Toluene |
| form | powder to crystal |
| color | White to Almost white |
| InChI | InChI=1S/C25H17Br/c26-20-12-8-11-19(17-20)25(18-9-2-1-3-10-18)23-15-6-4-13-21(23)22-14-5-7-16-24(22)25/h1-17H |
| InChIKey | LWBYEDXZPBXTFL-UHFFFAOYSA-N |
| SMILES | C1(C2=CC=CC(Br)=C2)(C2=CC=CC=C2)C2=C(C=CC=C2)C2=C1C=CC=C2 |
| CAS DataBase Reference | 1257251-75-4 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 |
| HS Code | 2903.99.8001 |
9-(3-Bromophenyl)-9-phenyl-9H-fluorene price More Price(19)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | B5616 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene >98.0%(GC) | 1257251-75-4 | 1g | $79 | 2026-04-30 | Buy |
| TCI Chemical | B5616 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene >98.0%(GC) | 1257251-75-4 | 5g | $240 | 2026-04-30 | Buy |
| Biosynth | HAC25175 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene | 1257251-75-4 | 5g | $900 | 2026-06-04 | Buy |
| Biosynth | HAC25175 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene | 1257251-75-4 | 50g | $900 | 2026-06-04 | Buy |
| Biosynth | HAC25175 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene | 1257251-75-4 | 2g | $900 | 2026-06-04 | Buy |
9-(3-Bromophenyl)-9-phenyl-9H-fluorene Chemical Properties, Uses, Production
Uses
9-(3-Bromophenyl)-9-phenyl-9H-fluorene is a useful research chemical.
Description
9-(3-Bromophenyl)-9-phenyl-9H-fluorene (9-(3-bromophenyl)-9-phenylfluorene) is an important organic intermediate to synthetize its substituted products.
Synthesis
A solution of 10.0 g of 2-bromobiphenyl (42.9 mmol) in 70 ml of anhydrous THF was added to a 500 mE 3-neck flask and cooled to -78 C. 27 ml of a 1.58 M hexane solution of n-BuEi (42.9 mmol) was then added dropwise while stirring, and the reaction was stirred for about 2.5 hours. A solution of 9.30 g (35.6 mmol) of 3-bromobenzophenone in 85 mE of an anhydrous THF was added dropwise, and the resulting mixture was stirred for about 2 hours at -78 C. followed by stirring for about 3 hours at room temperature. 1 N hydrochloric acid (HC1) was then added to the mixture and stirred for about 1 hour. The mixture was washed with water, and the resultant organic phase was concentrated to afford a material having a candy-like consistency. The candy-like material, 50 ml of acetic acid, and 2.4 ml of hydrochloric acid were added to a 500 mL recovery flask, and the mixture was stirred and reacted at 130 C. under a nitrogen atmosphere for about 2 hours. After the reaction, the reaction mixture was added dropwise to 350 ml of ice-cold water, precipitating white crystals, and the crystals were isolated by filtration. The crystals were washed with methanol and allowed to dry. About 13.3 g of Compound A was obtained as a white powder (yield: about 78%).
9-(3-Bromophenyl)-9-phenyl-9H-fluorene Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Henan Chuangan Optoelectronics Technology Co., Ltd. | 61280670 13215992208 | hnchuangan.w@qq.com | China | 747 | 58 |
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| Beijing Isomersyn Technology CO;LTD | 010-82954736 13391601435 | sales@isomersyn.com | China | 3294 | 57 |
| Hunan Hui Bai Shi Biotechnology Co., Ltd. | 0731-85526065 13308475853 | ivy@hnhbsj.com | China | 7236 | 62 |
| Springchem New Material Technology Co.,Limited | +86-021-62885108 | info@spring-chem.com | China | 2068 | 57 |
| Yurui (Shanghai) Chemical Co., Ltd. | 02150456736 18602143071 | Jenny@riyngroup.com | China | 500 | 30 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 03-36680489 | Sales-JP@TCIchemicals.com | Japan | 28364 | 80 |
| TCI Europe | 320-37350700 | sales@tcieurope.eu | Europe | 23654 | 75 |
| TCI AMERICA | 800-4238616 | sales@tciamerica.com | Americas | 23636 | 75 |
| Zhengzhou HQ Material Co., Ltd. | 0371-67759225 13526468238 | 3165471285@qq.com | China | 510 | 60 |
Related articles
- Preparation of 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene (9-(3-bromophenyl)-9-phenylfluorene) is an important organic intermediate to synthetize....
- Nov 8,2019
View Latest Price from 9-(3-Bromophenyl)-9-phenyl-9H-fluorene manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2026-09-02 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
|
$1.00-200.00 | 1KG | 99%, 99.5% Sublimated | Henan Fengda Chemical Co., Ltd | ||
 |
2026-08-18 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
|
1KG | 98% | 150KG /month | Shanghai Daken Advanced Materials Co.,Ltd | ||
 |
2026-01-20 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
|
25kg | 99.8% | 100kg | Zhongwei Coking Technology National Engineering Research Center Co., Ltd. |
-
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
- $1.00-200.00
- 99%, 99.5% Sublimated
- Henan Fengda Chemical Co., Ltd
-
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
- $0.00
- 98%
- Shanghai Daken Advanced Materials Co.,Ltd
-
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
- $0.00
- 99.8%
- Zhongwei Coking Technology National Engineering Research Center Co., Ltd.
