2,6-DICHLOROPHENYLBORONIC ACID
- CAS No.
- 73852-17-2
- Chemical Name:
- 2,6-DICHLOROPHENYLBORONIC ACID
- Synonyms
- AKOS BRN-0086;RARECHEM AH PB 0089;2,6-DICHLOROPHENYLBO;2,6-Dichlorophenylboronic;3,6-DICHLOROPHENYLBORONICACID;2,6-Dichlorobenzeneboronicaci;2,6-DICHLOROPHENYLBORONIC ACID;2,6-DICHLOROBENZENEBORONIC ACID;2,6-Dichlorophenylboronic acid,98%;B-(2,6-Dichlorophenyl)boronic acid
- CBNumber:
- CB1435113
- Molecular Formula:
- C6H5BCl2O2
- Molecular Weight:
- 190.82
- MDL Number:
- MFCD00064869
- MOL File:
- 73852-17-2.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Product description | Number | Pack Size | Price |
| 2,6-Dichlorophenylboronic Acid (contains varying amounts of Anhydride) | D3357 | 1g | $38 |
| 2,6-Dichlorophenylboronic Acid (contains varying amounts of Anhydride) | D3357 | 5g | $150 |
| 2,6-Dichlorophenylboronic acid 96-105%(Assaybytitration) | 40204 | 1G | $18.53 |
| 2,6-Dichlorophenylboronic acid 96-105%(Assaybytitration) | 40204 | 5G | $40.76 |
| 2,6-Dichlorophenylboronic acid | 005593 | 25.00g | $34 |
| More product size | |||
| Melting point | 153 °C |
|---|---|
| Boiling point | 341.8±52.0 °C(Predicted) |
| Density | 1.47±0.1 g/cm3(Predicted) |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| form | Powder |
| pka | 7.94±0.58(Predicted) |
| color | Off-white |
| Water Solubility | Insoluble in water. |
| BRN | 4802506 |
| CAS DataBase Reference | 73852-17-2(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H335-H315-H319 | |||||||||
| Precautionary statements | P261-P280a-P304+P340-P305+P351+P338-P405-P501a-P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 | |||||||||
| Hazard Codes | Xi,Xn | |||||||||
| Risk Statements | 36/37/38-22-36 | |||||||||
| Safety Statements | 26-36-37/39 | |||||||||
| HazardClass | IRRITANT | |||||||||
| HS Code | 29319090 | |||||||||
| NFPA 704 |
|
2,6-DICHLOROPHENYLBORONIC ACID price More Price(60)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | D3357 | 2,6-Dichlorophenylboronic Acid (contains varying amounts of Anhydride) | 73852-17-2 | 1g | $38 | 2026-04-30 | Buy |
| TCI Chemical | D3357 | 2,6-Dichlorophenylboronic Acid (contains varying amounts of Anhydride) | 73852-17-2 | 5g | $150 | 2026-04-30 | Buy |
| Chem-Impex | 40204 | 2,6-Dichlorophenylboronic acid 96-105%(Assaybytitration) | 73852-17-2 | 1G | $18.53 | 2026-05-19 | Buy |
| Chem-Impex | 40204 | 2,6-Dichlorophenylboronic acid 96-105%(Assaybytitration) | 73852-17-2 | 5G | $40.76 | 2026-05-19 | Buy |
| Matrix Scientific | 005593 | 2,6-Dichlorophenylboronic acid | 73852-17-2 | 25.00g | $34 | 2026-05-18 | Buy |
2,6-DICHLOROPHENYLBORONIC ACID Chemical Properties,Uses,Production
Chemical Properties
Off-white Cryst
Uses
suzuki reaction
Uses
Reagent used for palladium-catalyzed stille and suzuki-miyaura cross-couplings, palladium (pd)-catalytized reactions. Reagent used in preparation of common building blocks for pharmaceuticals and agrochemicals.
Synthesis
688-74-4
541-73-1
73852-17-2
(1) Lithiation reaction: Add 50 g of 1,3-dichlorobenzene to a 1000 mL three-necked flask under nitrogen atmosphere and cool to -80 to -60°C. Slowly add 176 mL of n-butyl lithium (n-BuLi) dropwise. Slowly add 176 mL of n-Butyl lithium (n-BuLi) dropwise and keep the reaction temperature between -80 and -50℃. After the dropwise addition, the reaction was continued for 2 hours. (2) Lithium-hydrogen exchange reaction: 117 g of tributyl borate (B(OBu)3) was added dropwise to the phenyl lithium solution prepared above, and the reaction temperature was maintained at a holding temperature after the dropwise addition was completed. At the end of the reaction, 10% hydrochloric acid solution was added to the system for acidification, stirred and left to stratify. The organic layers were separated, combined and the solvent was removed, and treated with hydrated succinamide to obtain 51.7 g of crude 2,6-dichlorophenylboronic acid in 80% yield. (3) Purification step: 51.7 g of crude 2,6-dichlorophenylboronic acid was placed in a 1 L three-necked flask and dissolved by adding 200 mL of methyl tert-butyl ether (MTBE). After removing the solvent, cooled and crystallized, centrifuged to obtain 48.4 g of pure 2,6-dichlorophenylboronic acid in 75% yield.
References
[1] Patent: CN108084217, 2018, A. Location in patent: Paragraph 0006; 0017-0020; 0022-0024; 0026-0028; 0030-0032
2,6-DICHLOROPHENYLBORONIC ACID Preparation Products And Raw materials
Raw materials
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Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Capot Chemical Co.,Ltd. | +8613336195806 | sales@capot.com | China | 29640 | 60 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-2158073036 | info@dakenam.com | China | 13901 | 58 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29815 | 58 |
| Jinan Finer Chemical Co., Ltd | +86-531-88989536 +86-15508631887 | sales@finerchem.com | China | 2950 | 58 |
| Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 21193 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Wuhan Chemwish Technology Co., Ltd | 027-67849912 | sales@chemwish.com | CHINA | 10821 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49979 | 58 |
| Richest Group Ltd | 18017061086 | oled@richest-group.com | CHINA | 5600 | 58 |
View Lastest Price from 2,6-DICHLOROPHENYLBORONIC ACID manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2026-05-21 | 2,6-Dichlorophenylboronic acid
73852-17-2
|
$5.00 | 1kg | ≥99% | 200mt/year | Jinan Finer Chemical Co., Ltd | |
 |
2021-07-13 | 2,6-DICHLOROPHENYLBORONIC ACID
73852-17-2
|
$10.00-15.00 | 1KG | 99%+ HPLC | Zhuozhou Wenxi import and Export Co., Ltd | ||
 |
2021-07-10 | 2,6-DICHLOROPHENYLBORONIC ACID
73852-17-2
|
$10.00-15.00 | 1KG | 99%+ HPLC | Zhuozhou Wenxi import and Export Co., Ltd |
-
- 2,6-Dichlorophenylboronic acid
73852-17-2
- $5.00
- ≥99%
- Jinan Finer Chemical Co., Ltd
-
- 2,6-DICHLOROPHENYLBORONIC ACID
73852-17-2
- $10.00-15.00
- 99%+ HPLC
- Zhuozhou Wenxi import and Export Co., Ltd
-
- 2,6-DICHLOROPHENYLBORONIC ACID
73852-17-2
- $10.00-15.00
- 99%+ HPLC
- Zhuozhou Wenxi import and Export Co., Ltd
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