Methyl 2-amino-5-bromo-3-iodobenzoate
- CAS No.
- 289039-83-4
- Chemical Name:
- Methyl 2-amino-5-bromo-3-iodobenzoate
- Synonyms
- Methyl 2-amino-3-iodo-5-bromobenzoate;Methyl 2-amino-5-bromo-3-iodobenzoate;2-Amino-5-bromo-3-iodo-benzoic acid methyl ester;Methyl 2-amino-5-bromo-3-iodobenzoate - [M71779];Benzoic acid, 2-amino-5-bromo-3-iodo-, methyl ester
- CBNumber:
- CB1461987
- Molecular Formula:
- C8H7BrINO2
- Molecular Weight:
- 355.96
- MDL Number:
- MFCD00673015
- MOL File:
- 289039-83-4.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302 |
| Precautionary statements | P280-P305+P351+P338 |
Methyl 2-amino-5-bromo-3-iodobenzoate price More Price(23)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Matrix Scientific | 096031 | Methyl 2-amino-5-bromo-3-iodobenzoate | 289039-83-4 | 250.00mg | $265 | 2026-05-18 | Buy |
| Matrix Scientific | 096031 | Methyl 2-amino-5-bromo-3-iodobenzoate | 289039-83-4 | 1.00g | $588 | 2026-05-18 | Buy |
| Synthonix | M71779 | Methyl 2-amino-5-bromo-3-iodobenzoate 97% | 289039-83-4 | 250mg | $16 | 2026-05-06 | Buy |
| Synthonix | M71779 | Methyl 2-amino-5-bromo-3-iodobenzoate 97% | 289039-83-4 | 1g | $20 | 2026-05-06 | Buy |
| Synthonix | M71779 | Methyl 2-amino-5-bromo-3-iodobenzoate 97% | 289039-83-4 | 5g | $100 | 2026-05-06 | Buy |
Methyl 2-amino-5-bromo-3-iodobenzoate Chemical Properties, Uses, Production
Synthesis
52727-57-8
289039-83-4
General procedure for the synthesis of methyl 2-amino-5-bromo-3-iodobenzoate from methyl 5-bromoaminobenzoate: 371 mg of methyl 2-amino-5-bromobenzoate (2 mmol) was dissolved in 2 mL of concentrated acetic acid, and 495 mg of N-iodosuccinimide (2.2 mmol) was added and the reaction was carried out for 17 hours at room temperature. After completion of the reaction, the mixture was poured into a mixture of 5 mL of saturated sodium bicarbonate solution and ice and extracted twice with ethyl acetate (EtOAc). The organic phases were combined, washed with saturated brine, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to give 585 mg of methyl 2-amino-5-bromo-3-iodobenzoate (82% yield) as a light brown solid. Mass spectrometry (EI) showed a molecular ion peak m/z 354.9 (M+).
References
[1] Patent: US2006/30613, 2006, A1. Location in patent: Page/Page column 21-22
[2] Patent: WO2016/87975, 2016, A1. Location in patent: Page/Page column 26
Methyl 2-amino-5-bromo-3-iodobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Methyl 2-amino-5-bromo-3-iodobenzoate Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| PharmaBlock Sciences (Nanjing),Inc. | 025-86918202 4000255188 | sales@pharmablock.com | China | 5000 | 55 |
| SuZhou ShiYa Biopharmaceuticals, Inc. | 0512-0512-52358471 17715136450 | sales@shiyabiopharm.com | China | 9814 | 58 |
| Tianjin Kailiqi Biotechnology Co., Ltd. | 15076683720 | klq@cw-bio.com | China | 9780 | 55 |
| Suzhou JingTong Pharmaceutical Co., Ltd. | 13675155016 | tongtf110@sina.com | China | 963 | 55 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Aikon International Limited | 025-58859352 13913916777 | dt3@aikonchem.com | China | 15490 | 58 |
| Suzhou Nuoouman Biological Technology Co., Ltd. | 15026866316 | 180642609@qq.com | China | 4966 | 58 |
| Suzhou Xiya Pharmaceutical Co., Ltd. | 0512-87819718 18912655635 | 2587879032@qq.com | China | 1275 | 58 |
| Nanjing SynTitan Pharmaceutical Co., Ltd. | 025-57027686 17372956142 | li_lan@syntitan.com | China | 9999 | 58 |
| Shanghai Changer Pharmaceutical Technology Co. Ltd. | 15921595598;15921595598 | qd.yu@pharmachanger.com | China | 469 | 58 |
