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2-METHOXY-5-NITROBENZALDEHYDE

2-METHOXY-5-NITROBENZALDEHYDE Structure
2-METHOXY-5-NITROBENZALDEHYDE structure
CAS No.
25016-02-8
Chemical Name:
2-METHOXY-5-NITROBENZALDEHYDE
Synonyms
AKOS B028867;5-Nitro-o-anisaldehyde;5-Nitro-o-anisaldehyde;2-METHOXY-5-NITROBENZALDEHYDE;2-methoxy-5-nitro-benzaldehyd;Benzaldehyde, 2-methoxy-5-nitro-;4-(4-morpholinyl)-6-[[4-(phenylmethyl)-1-piperazinyl]methyl]-1,3,5-triazin-2-amine
CBNumber:
CB1676781
Molecular Formula:
C8H7NO4
Molecular Weight:
181.15
MDL Number:
MFCD02093683
MOL File:
25016-02-8.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:48
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2-METHOXY-5-NITROBENZALDEHYDE Properties

Melting point 89-92 °C (lit.)
Boiling point 336.7±27.0 °C(Predicted)
Density 1.322±0.06 g/cm3(Predicted)
storage temp. Inert atmosphere,Room Temperature
solubility very soluble in Dimethylformamide
form powder to crystal
color White to Light yellow to Light orange
CAS DataBase Reference 25016-02-8
EPA Substance Registry System Benzaldehyde, 2-methoxy-5-nitro- (25016-02-8)
UNSPSC Code 12352100
NACRES NA.22

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313
WGK Germany  3
HS Code  2913000090

2-METHOXY-5-NITROBENZALDEHYDE price More Price(28)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 515760 2-Methoxy-5-nitrobenzaldehyde 97% 25016-02-8 5g $296 2022-05-15 Buy
TCI Chemical N1034 5-Nitro-o-anisaldehyde min. 98.0 % 25016-02-8 5G $36 2025-07-31 Buy
TCI Chemical N1034 5-Nitro-o-anisaldehyde min. 98.0 % 25016-02-8 25G $108 2025-07-31 Buy
AK Scientific J94624 2-Methoxy-5-nitrobenzaldehyde 25016-02-8 5g $119 2021-12-16 Buy
AK Scientific 1946AB 2-Methoxy-5-nitrobenzaldehyde 25016-02-8 5g $149 2021-12-16 Buy
Product number Packaging Price Buy
515760 5g $296 Buy
N1034 5G $36 Buy
N1034 25G $108 Buy
J94624 5g $119 Buy
1946AB 5g $149 Buy

2-METHOXY-5-NITROBENZALDEHYDE Chemical Properties,Uses,Production

Synthesis

5-Nitrosalicylaldehyde

97-51-8

Iodomethane

74-88-4

2-METHOXY-5-NITROBENZALDEHYDE

25016-02-8

General procedure for the synthesis of 2-methoxy-5-nitrobenzaldehyde from 5-nitrosalicylaldehyde and iodomethane: Sodium hydride (NaH, 246 mg) and iodomethane (2.56 g) were added to a solution of 5-nitrosalicylaldehyde (1.00 g, 6.0 mmol) in N,N-dimethylformamide (DMF, 20 ml). The reaction mixture was stirred at 0°C for 8.5 hours. After completion of the reaction, the reaction mixture was extracted with ether and the organic phase was washed sequentially with aqueous sodium bicarbonate, saturated brine and 5% hydrochloric acid/saturated brine. The organic phase was dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give 2-methoxy-5-nitrobenzaldehyde (0.95 g, 87.8% yield) as yellow needle-like crystals. The product was characterized by 1H NMR (CDCl3): δ 10.45 (s, 1H), 8.70 (d, J = 2.9Hz, 1H), 8.45 (dd, J = 8.8, 2.9Hz, 1H), 7.14 (d, J = 8.8Hz, 1H), 4.08 (s, 3H).

References

[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 15, p. 3435 - 3438
[2] Patent: US2013/261295, 2013, A1. Location in patent: Paragraph 0166; 0167
[3] Journal of the American Chemical Society, 2017, vol. 139, # 19, p. 6654 - 6662
[4] Patent: US5837711, 1998, A
[5] Journal of the Chemical Society, 1951, p. 2462,2466

2-METHOXY-5-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Silver oxide Diethyl ether 5-Nitrosalicylaldehyde Methanol Iodomethane
2-methoxy-5-nitrobenzonitrile Sodium hydride N,N-Dimethylformamide

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Preparation Products

2-METHOXY-5-NITROBENZALDEHYDE Suppliers

Global( 94)Suppliers
Supplier Tel Email Country ProdList Advantage
CONIER CHEM AND PHARMA LIMITED 		+8618523575427 sales@conier.com China 49975 58
Shaanxi Dideu Medichem Co. Ltd 		+86-29-87569262 +86-15003564040 1087@dideu.com China 3958 58
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd 		+8613580539051 joe@yuhengpharm.com CHINA 21142 58
Hefei TNJ Chemical Industry Co.,Ltd. 		+86-0551-65418671 +8618949823763 sales@tnjchem.com China 34563 58
Win-Win chemical CO., Limited 		+86-0086-577-64498589 +86-15355981851 sales@win-winchemical.com China 14360 58
Dayang Chem (Hangzhou) Co.,Ltd. 		+86-0571-88938639 +8617705817739 info@dycnchem.com China 52846 58
Aromsyn Co., Ltd. 		+86-0571-85585865 +8613336024896 CB@aromsyn.com China 19183 58
PT CHEM GROUP LIMITED 		+86-85511178; peter68@ptchemgroup.com China 35425 58
GIHI CHEMICALS CO.,LIMITED 		+8618058761490 info@gihichemicals.com China 49977 58
Aceschem Inc. 		+1-817863-6948 +1-（817）863-6948 sales@aceschem.com United States 19632 58
Supplier Advantage
CONIER CHEM AND PHARMA LIMITED 		58
Shaanxi Dideu Medichem Co. Ltd 		58
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd 		58
Hefei TNJ Chemical Industry Co.,Ltd. 		58
Win-Win chemical CO., Limited 		58
Dayang Chem (Hangzhou) Co.,Ltd. 		58
Aromsyn Co., Ltd. 		58
PT CHEM GROUP LIMITED 		58
GIHI CHEMICALS CO.,LIMITED 		58
Aceschem Inc. 		58

View Lastest Price from 2-METHOXY-5-NITROBENZALDEHYDE manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2-Methoxy-5-nitrobenzaldehyde pictures 2025-01-03 2-Methoxy-5-nitrobenzaldehyde
25016-02-8
 US $0.00-0.00 / KG 10mg 99%HPLC 2000tons Shaanxi Dideu Medichem Co. Ltd

2-METHOXY-5-NITROBENZALDEHYDE Spectrum

2-METHOXY-5-NITROBENZALDEHYDE(25016-02-8)1HNMR2-METHOXY-5-NITROBENZALDEHYDE(25016-02-8)IR

25016-02-8(2-METHOXY-5-NITROBENZALDEHYDE)Related Search:

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5-METHOXY-2-NITROBENZALDEHYDE 4-METHOXY-3-NITROBENZALDEHYDE 3-METHOXY-2-NITROBENZALDEHYDE,3-METHOXY-2-NITROBENZALDEHYDE, 97+% 2-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE 98%,2-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE 2-(4-METHOXYPHENOXY)-5-NITROBENZOIC ACID
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2-methoxy-5-nitro-benzaldehyd AKOS B028867 2-METHOXY-5-NITROBENZALDEHYDE Benzaldehyde, 2-methoxy-5-nitro- 5-Nitro-o-anisaldehyde 5-Nitro-o-anisaldehyde 4-(4-morpholinyl)-6-[[4-(phenylmethyl)-1-piperazinyl]methyl]-1,3,5-triazin-2-amine 25016-02-8 Carbonyl Compounds C8 Building Blocks Aldehydes Organic Building Blocks Aldehydes C8 Carbonyl Compounds