DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE
- CAS No.
- 76535-75-6
- Chemical Name:
- DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE
- Synonyms
- 1,4-Bis(Boc)piperazine;DI-TERT-BUTYLPIPERAZINE-1;1,4-Bis(tert-butoxycarbonyl)piperazine;1,4-Bis (t-butyloxycarbonyl) piperazine;DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE;1,4-Di-tert-butyl piperazine-1,4-dicarboxylate;1,4-piperazinedicarboxylic acid, bis(1,1-dimethylethyl) ester;1,4-Piperazinedicarboxylic acid, 1,4-bis(1,1-dimethylethyl) ester
- CBNumber:
- CB21229864
- Molecular Formula:
- C14H26N2O4
- Molecular Weight:
- 286.37
- MDL Number:
- MFCD01435774
- MOL File:
- 76535-75-6.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 1,4-Di-tert-butyl piperazine-1,4-dicarboxylate | 411288 | 100mg | $305 |
| Di(tert-butyl) 1,4-piperazinedicarboxylate | 173384 | 1g | $316 |
| 1,4-Di-tert-butyl piperazine-1,4-dicarboxylate | FD43643 | 50g | $375 |
| 1,4-Di-tert-butyl piperazine-1,4-dicarboxylate | FD43643 | 10g | $146.6 |
| 1,4-Di-tert-butylpiperazine-1,4-dicarboxylate | B999 | 1g | $20 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE price More Price(30)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Usbiological | 411288 | 1,4-Di-tert-butyl piperazine-1,4-dicarboxylate | 76535-75-6 | 100mg | $305 | 2021-12-16 | Buy |
| Matrix Scientific | 173384 | Di(tert-butyl) 1,4-piperazinedicarboxylate | 76535-75-6 | 1g | $316 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FD43643 | 1,4-Di-tert-butyl piperazine-1,4-dicarboxylate | 76535-75-6 | 50g | $375 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FD43643 | 1,4-Di-tert-butyl piperazine-1,4-dicarboxylate | 76535-75-6 | 10g | $146.6 | 2021-12-16 | Buy |
| AK Scientific | B999 | 1,4-Di-tert-butylpiperazine-1,4-dicarboxylate | 76535-75-6 | 1g | $20 | 2021-12-16 | Buy |
DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE Chemical Properties,Uses,Production
Synthesis
110-85-0
24424-99-5
76535-75-6
General procedure for the synthesis of 1,4-bis(tert-butoxycarbonyl)piperazine from piperazine and di-tert-butyl dicarbonate: In a 10 mL round bottom flask, EtOH (5 mL), di-tert-butyl dicarbonate (1-2 mmol), nano-Fe3O4 catalyst (3 mol%, 0.007 g) and piperazine (1 mmol) were added. The reaction mixture was stirred at room temperature until complete (refer to Table 3 for reaction times). After completion of the reaction, the nano-Fe3O4 catalyst was separated using external magnet adsorption. The separated solution was dried and the solvent was concentrated, and the resulting crude product was recrystallized with hexane or ethyl acetate (5 mL) to give pure 1,4-bis(tert-butoxycarbonyl)piperazine. The recovered Fe3O4 nanocatalyst was washed with EtOH and dried, and could be reused. The catalyst was recycled six times without significant changes in the reaction yield and time.
References
[1] Tetrahedron Letters, 2009, vol. 50, # 46, p. 6244 - 6246
[2] Synthetic Communications, 2012, vol. 42, # 1, p. 25 - 32
[3] Tetrahedron Letters, 2007, vol. 48, # 47, p. 8318 - 8322
[4] Comptes Rendus Chimie, 2013, vol. 16, # 11, p. 962 - 966
[5] Chinese Journal of Catalysis, 2013, vol. 34, # 9, p. 1730 - 1733
DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE Preparation Products And Raw materials
DI-TERT-BUTYLPIPERAZINE-1,4-DICARBOXYLATE Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| sgtlifesciences pvt ltd | +8617013299288 | dj@sgtlifesciences.com | China | 12373 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 57505 | 58 | |
| Moxin Chemicals | +86-17320513646 +8617320513646 | anna@molcoo.com | China | 10000 | 58 |
| ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD | +86-13017695106 +86-13676922317 | jiuyitime@fdachem.com | China | 16516 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Energy Chemical | 021-021-58432009 400-005-6266 | sales8178@energy-chemical.com | China | 44733 | 61 |
| Pure Chemistry Scientific Inc. | 001-857-928-2050 or 1-888-588-9418 | sales@chemreagents.com | United States | 10186 | 62 |
| Adamas Reagent, Ltd. | 400-6009262 16621234537 | chenyj@titansci.com | China | 14101 | 59 |
| 9ding chemical ( Shanghai) Limited | 4009209199 | sales@9dingchem.com | China | 18209 | 56 |
| Shanghai Aladdin Bio-Chem Technology Co.,LTD | 400-6206333 13167063860 | anhua.mao@aladdin-e.com | China | 25003 | 65 |
