(3-AMINO-5-NITROPHENYL)METHANOL
- CAS No.
- 90390-46-8
- Chemical Name:
- (3-AMINO-5-NITROPHENYL)METHANOL
- Synonyms
- 3-Amino-5-nitrobenzenemethanol;(3-AMINO-5-NITROPHENYL)METHANO;(3-AMINO-5-NITROPHENYL)METHANOL;3-(Hydroxymethyl)-5-nitroaniline;Benzenemethanol, 3-amino-5-nitro-
- CBNumber:
- CB2377203
- Molecular Formula:
- C7H8N2O3
- Molecular Weight:
- 168.15
- MDL Number:
- MFCD08236778
- MOL File:
- 90390-46-8.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| (3-Amino-5-nitrophenyl)methanol 98% | AS32513 | 1g | $72 |
| (3-Amino-5-nitrophenyl)methanol 98% | AS32513 | 5g | $309 |
| (3-Amino-5-nitrophenyl)methanol | 074465 | 250.00mg | $260 |
| (3-Amino-5-nitrophenyl)methanol | 074465 | 1.00g | $559 |
| (3-Amino-5-nitrophenyl)methanol | 074465 | 5.00g | $1519 |
| More product size | |||
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H332-H335 |
| Precautionary statements | P261-P280-P305+P351+P338 |
(3-AMINO-5-NITROPHENYL)METHANOL price More Price(35)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS32513 | (3-Amino-5-nitrophenyl)methanol 98% | 90390-46-8 | 1g | $72 | 2026-06-04 | Buy |
| Activate Scientific | AS32513 | (3-Amino-5-nitrophenyl)methanol 98% | 90390-46-8 | 5g | $309 | 2026-06-04 | Buy |
| Matrix Scientific | 074465 | (3-Amino-5-nitrophenyl)methanol | 90390-46-8 | 250.00mg | $260 | 2026-05-18 | Buy |
| Matrix Scientific | 074465 | (3-Amino-5-nitrophenyl)methanol | 90390-46-8 | 1.00g | $559 | 2026-05-18 | Buy |
| Matrix Scientific | 074465 | (3-Amino-5-nitrophenyl)methanol | 90390-46-8 | 5.00g | $1519 | 2026-05-18 | Buy |
(3-AMINO-5-NITROPHENYL)METHANOL Chemical Properties,Uses,Production
Synthesis
71022-43-0
90390-46-8
(ii) Synthesis of 3-amino-5-nitrobenzyl alcohol: 3,5-dinitrobenzyl alcohol (129.1 g, 0.65 mol) from step (i) was dissolved in methanol (1500 mL) and heated to reflux. Ammonium sulfide solution (450 mL, containing 20 wt% H2O, 442.9 g, 1.30 mol) was added slowly over 45 min. The resulting non-homogeneous mixture was refluxed for 2 hours, followed by stirring at 25 °C for 18 hours. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad and the filtrate was acidified with 2N hydrochloric acid and the methanol was evaporated under reduced pressure. The remaining acidic aqueous solution was washed with ether (3×) and then alkalized with 6N sodium hydroxide solution. The alkalized aqueous solution was extracted with ether (4×). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 95.8 g (88% yield) of 3-amino-5-nitrobenzenemethanol as an orange solid, which could be used in the next reaction without further purification. The product was characterized by 1H NMR (300 MHz, CD3OD): δ 7.46 (m, 1H), 7.38 (m, 1H), 6.98 (m, 1H), 4.57 (s, 2H).
References
[1] Tetrahedron Letters, 2003, vol. 44, # 29, p. 5477 - 5481
[2] Chinese Chemical Letters, 2011, vol. 22, # 7, p. 785 - 788
[3] Journal of Medicinal Chemistry, 1984, vol. 27, # 9, p. 1111 - 1118
[4] Bioorganic and medicinal chemistry letters, 2002, vol. 12, # 22, p. 3263 - 3265
[5] Journal of Labelled Compounds and Radiopharmaceuticals, 2002, vol. 45, # 3, p. 257 - 268
(3-AMINO-5-NITROPHENYL)METHANOL Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Wuhan Chemwish Technology Co., Ltd | 027-67849912 | sales@chemwish.com | CHINA | 10821 | 58 |
| Kindchem(Nanjing)Co.,Ltd | +86-025-025-85281586 +8618651653755 | sales@kindchem.cn | China | 1226 | 58 |
| Henan Alfa Chemical Co., Ltd | +8615838112936 | sale03@alfachem.cn | China | 9796 | 58 |
| Sichuan Biosynce Pharmatech Co., Ltd. | +8619950309693 | diane@biosynce.com | China | 4871 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| DAYANG CHEM (HANGZHOU) CO.,LTD | +86-88938639 +86-17705817739 | info@dycnchem.com | China | 53803 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Wuhan Chemwish Technology Co., Ltd | 86-027-67849912 | sales@chemwish.com | China | 35896 | 56 |
90390-46-8((3-AMINO-5-NITROPHENYL)METHANOL)Related Search:
1of4
