METHYL PHENYL CARBONATE
- CAS No.
- 13509-27-8
- Chemical Name:
- METHYL PHENYL CARBONATE
- Synonyms
- Benzoyl carbonate;PHENYLMETHYL CARBONATE;METHYL PHENYL CARBONATE;Carbonic acid methyl phenyl;Carbonic acid=methyl=phenyl ester;Carbonic acid O-phenyl O-methyl ester
- CBNumber:
- CB2712514
- Molecular Formula:
- C8H8O3
- Molecular Weight:
- 152.15
- MDL Number:
- MFCD04039782
- MOL File:
- 13509-27-8.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P280a-P304+P340-P305+P351+P338-P405-P501a | |||||||||
| Safety Statements | 22-24/25 | |||||||||
| NFPA 704 |
|
METHYL PHENYL CARBONATE price More Price(11)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AK Scientific | 9802CA | Methylphenylcarbonate | 13509-27-8 | 10g | $157 | 2021-12-16 | Buy |
| AK Scientific | 9802CA | Methylphenylcarbonate | 13509-27-8 | 1g | $77 | 2021-12-16 | Buy |
| Ambeed | A189967 | Methylphenylcarbonate 98% | 13509-27-8 | 25g | $116 | 2021-12-16 | Buy |
| Chemenu | CM248967 | Methylphenylcarbonate 95+% | 13509-27-8 | 25g | $143 | 2021-12-16 | Buy |
| Chemenu | CM248967 | Methylphenylcarbonate 95+% | 13509-27-8 | 100g | $402 | 2021-12-16 | Buy |
METHYL PHENYL CARBONATE Chemical Properties,Uses,Production
Chemical Properties
colourless liquid
Synthesis
67-56-1
1202680-24-7
13509-27-8
GENERAL METHODS: To a solution of methanol (0.7 mmol) and AlCl3 (0.7 mmol) in toluene (10 mL) was added compound 3 (CAS:1202680-24-7, 0.7 mmol). The progress of the reaction was monitored by thin layer chromatography (TLC) and the mixture was stirred at room temperature until the compound 3 was completely consumed. Upon completion of the reaction, 10% NaOH aqueous solution (50 mL) and dichloromethane (30 mL) were added to the reaction mixture under stirring for extraction. The organic layer was separated and washed with distilled water (50 mL) and subsequently dried over anhydrous magnesium sulfate. The solvent was removed by evaporation under reduced pressure to give the crude product. The crude product was purified by passing through an open silica gel column (2.5 x 4 cm) using hexane/ethyl acetate (3:1, v/v) as eluent. Compounds 5 and 6 were eluted first, followed by ethyl acetate. Finally, 4,5-dichloropyridazin-3(2H)-one (1) was eluted. The column chromatography fractions containing the pure compounds were combined and the solvents were evaporated under reduced pressure to afford the target product, methyl phenyl carbonate.4,5-Dichloropyridazin-3(2H)-one was obtained in quantitative yield and was reusable.
References
[1] Bulletin of the Korean Chemical Society, 2014, vol. 35, # 9, p. 2758 - 2764
[2] Synlett, 2016, vol. 27, # 10, p. 1577 - 1581
METHYL PHENYL CARBONATE Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
METHYL PHENYL CARBONATE Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
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