N-Hexadecylbenzamide
- CAS No.
- 82684-41-1
- Chemical Name:
- N-Hexadecylbenzamide
- Synonyms
- N-Hexadecylbenzamide;Benzamide, N-hexadecyl-
- CBNumber:
- CB42391397
- Molecular Formula:
- C23H39NO
- Molecular Weight:
- 345.56
- MDL Number:
- MFCD03193479
- MOL File:
- 82684-41-1.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| N-Hexadecylbenzamide 95+% | 095338 | 1g | $152 |
| N-Hexadecylbenzamide | 2777AC | 250mg | $167 |
| N-Hexadecylbenzamide | 2777AC | 1g | $212 |
| N-Hexadecylbenzamide 95+% | 095338 | 5g | $404 |
| N-HEXADECYLBENZAMIDE 95.00% | CHM0393609 | 5MG | $504.47 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |   GHS07,GHS09 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H317-H410 |
| Precautionary statements | P501-P261-P273-P272-P270-P264-P280-P302+P352-P391-P362+P364-P333+P313-P301+P312+P330 |
N-Hexadecylbenzamide price More Price(11)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Matrix Scientific | 095338 | N-Hexadecylbenzamide 95+% | 82684-41-1 | 1g | $152 | 2021-12-16 | Buy |
| AK Scientific | 2777AC | N-Hexadecylbenzamide | 82684-41-1 | 250mg | $167 | 2021-12-16 | Buy |
| AK Scientific | 2777AC | N-Hexadecylbenzamide | 82684-41-1 | 1g | $212 | 2021-12-16 | Buy |
| Matrix Scientific | 095338 | N-Hexadecylbenzamide 95+% | 82684-41-1 | 5g | $404 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | CHM0393609 | N-HEXADECYLBENZAMIDE 95.00% | 82684-41-1 | 5MG | $504.47 | 2021-12-16 | Buy |
N-Hexadecylbenzamide Chemical Properties,Uses,Production
Synthesis
143-27-1
98-88-4
82684-41-1
The general procedure for the synthesis of N-hexadecylbenzamide from hexadecylamine and benzoyl chloride was as follows: benzoyl chloride (13.0 mL, 112 mmol) was dissolved in dichloromethane (200 mL) and the solution was cooled to 0°C in an ice bath. A second solution prepared from 1-hexadecylamine (30.8 g, 110 mmol) and triethylamine (17.0 mL, 122 mmol) in methylene chloride (300 mL) was added slowly and dropwise under nitrogen protection. The reaction mixture was stirred overnight at room temperature. Subsequently, the reaction products were washed sequentially with 10% aqueous hydrochloric acid solution (ethanol was added to avoid emulsification), saturated sodium bicarbonate solution and saturated sodium chloride solution. The organic phase was dried over anhydrous sodium sulfate and filtered, and dichloromethane was removed by evaporation under reduced pressure to give the white solid product N-hexadecylbenzamide (30.1 g, 87.0 mmol, 93% yield). The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3) and HRMS (ESI+): 1H NMR δ= 7.75 (d, J = 8.4 Hz, 2H), 7.49 (t, J = 6.7 Hz, 1H), 7.42 (t, J = 7.3 Hz, 2H), 6.14 (s, 1H), 3.44 (dd, J = 13.1, 7.0 Hz, 2H), 1.74-1.50 (m, 2H), 1.25 (s, 26H), 0.88 (t, J = 6.8 Hz, 3H); HRMS (ESI+) C23H40NO [M + H]+: calculated value 346.3104, measured value 346.3107.
References
[1] Tetrahedron Letters, 2011, vol. 52, # 32, p. 4215 - 4217
[2] Journal of Organic Chemistry, 2006, vol. 71, # 26, p. 9622 - 9627
N-Hexadecylbenzamide Preparation Products And Raw materials
Raw materials
Preparation Products
N-Hexadecylbenzamide Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Hangzhou MolCore BioPharmatech Co.,Ltd. | +86-057181025280; +8617767106207 | sales@molcore.com | China | 49734 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
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| Jiangsu Aikon Biopharmaceutical R&D co.,Ltd. | 025-66028182 18626450290 | yftan@aikonchem.com | China | 16676 | 50 |
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| ShangHai Angti Biotechnology Co., Ltd. | 13764913901 | info@angtibio.com | China | 4977 | 55 |
| Yantai ShengKailun Chemical Technology Co., Ltd. | 13356901049 | 3119594100@qq.com | China | 7964 | 55 |
| Changzhou Yinghao Technology Development Co., Ltd | 15151934985 | sales@yingsapharm.com | China | 5133 | 58 |
| Energy Chemical | 021-58432009 400-005-6266 | marketing@energy-chemical.com | China | 44918 | 58 |
| THchemica Co.,Ltd. | 0573-82835115 18969301519 | tly1019@126.com | China | 276 | 58 |
