N-Methoxy-N,2,2-trimethylpropanamide
- CAS No.
- 64214-60-4
- Chemical Name:
- N-Methoxy-N,2,2-trimethylpropanamide
- Synonyms
- N-Methoxy-N,2,2-trimethylpropanamide;Propanamide, N-methoxy-N,2,2-trimethyl-
- CBNumber:
- CB42565293
- Molecular Formula:
- C7H15NO2
- Molecular Weight:
- 145.2
- MDL Number:
- MFCD11847426
- MOL File:
- 64214-60-4.mol
| Product description | Number | Pack Size | Price |
| N-Methoxy-N,2,2-trimethylpropanamide | M268780 | 1g | $175 |
| N-Methoxy-N-methylpivalamide | 9831AB | 5g | $411 |
| N-Methoxy-N-methylpivalamide | 188534 | 5g | $478 |
| N-Methoxy-N-methylpivalamide | 188534 | 10g | $833 |
| N-Methoxy-N-methylpivalamide | 188534 | 25g | $1666 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302+H312+H332 |
| Precautionary statements | P501-P261-P270-P271-P264-P280-P362+P364-P301+P312+P330-P302+P352+P312-P304+P340+P312 |
| HS Code | 2928009090 |
N-Methoxy-N,2,2-trimethylpropanamide price More Price(8)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | M268780 | N-Methoxy-N,2,2-trimethylpropanamide | 64214-60-4 | 1g | $175 | 2021-12-16 | Buy |
| AK Scientific | 9831AB | N-Methoxy-N-methylpivalamide | 64214-60-4 | 5g | $411 | 2021-12-16 | Buy |
| Matrix Scientific | 188534 | N-Methoxy-N-methylpivalamide | 64214-60-4 | 5g | $478 | 2021-12-16 | Buy |
| Matrix Scientific | 188534 | N-Methoxy-N-methylpivalamide | 64214-60-4 | 10g | $833 | 2021-12-16 | Buy |
| Matrix Scientific | 188534 | N-Methoxy-N-methylpivalamide | 64214-60-4 | 25g | $1666 | 2021-12-16 | Buy |
N-Methoxy-N,2,2-trimethylpropanamide Chemical Properties,Uses,Production
Synthesis
1117-97-1
75-98-9
64214-60-4
GENERAL PROCEDURE: Methoxymethylamine (0.360 g, 6.0 mmol) and valproic acid (0.244 g, 2.0 mmol) were dissolved in anhydrous toluene (10 mL) and stirred for 10 min at 0 °C. Subsequently, a solution of phosphorus trichloride (0.137 g, 1.0 mmol) in anhydrous toluene (2 mL) was slowly added dropwise to the reaction mixture. After the dropwise addition, the reaction mixture was gradually warmed up to room temperature and stirring was continued for 0.5 h at 60 °C. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the completion of the reaction, the mixture was cooled to room temperature. The reaction was quenched with saturated sodium bicarbonate solution (20 mL) and subsequently extracted with ethyl acetate (3 x 10 mL). The organic phases were combined and dried over anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to give the crude product. The crude product was purified by column chromatography (silica gel, petroleum ether-ethyl acetate, 3:2) to afford N-methoxy-N,2,2-trimethylpropionamide (3a) as a colorless oil. Yield: 320 mg (97%).
References
[1] Synthesis (Germany), 2014, vol. 46, # 3, p. 320 - 330
[2] Journal of Organic Chemistry, 2004, vol. 69, # 25, p. 8984 - 8986
N-Methoxy-N,2,2-trimethylpropanamide Preparation Products And Raw materials
Raw materials
Preparation Products
N-Methoxy-N,2,2-trimethylpropanamide Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Career Henan Chemica Co | +86-0371-86658258 +8613203830695 | laboratory@coreychem.com | China | 30229 | 58 |
| AFINE CHEMICALS LIMITED | +86-0571-85134551 | sales@afinechem.com | China | 15089 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| Qingdao Dexin Chemical Co., Ltd | +86-15553333686 | 15553333686@qq.com | China | 3113 | 58 |
| Hebei Chuanghai Biotechnology Co., Ltd | +86-15350571055 | Sibel@chuanghaibio.com | China | 6085 | 58 |
| DAYANG CHEM (HANGZHOU) CO.,LTD | +86-88938639 +86-17705817739 | info@dycnchem.com | China | 53899 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Adamas Reagent, Ltd. | 400-6009262 16621234537 | chenyj@titansci.com | China | 14101 | 59 |
| Sci General Material & Chemical Ltd | 021-58388037;21-58388037 13472507714 | 35177634@qq.com;1589045147@qq.com | China | 806 | 55 |
