2-broMo-5-Methylpyridine-1-o×ide
- CAS No.
- 19230-58-1
- Chemical Name:
- 2-broMo-5-Methylpyridine-1-o×ide
- Synonyms
- 2-bromo-5-methylpyridine N-oxide;2-broMo-5-Methylpyridine-1-o×ide;Pyridine, 2-broMo-5-Methyl-, 1-oxide;2-bromo-5-methyl-1-oxidopyridin-1-ium;2-Bromo-5-methylpyridin-1-ium-1-olate
- CBNumber:
- CB52614141
- Molecular Formula:
- C6H6BrNO
- Molecular Weight:
- 188.02
- MDL Number:
- MFCD11052562
- MOL File:
- 19230-58-1.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | OR307223 | 250mg | $22 |
| 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | OR307223 | 1g | $49 |
| 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | OR307223 | 5g | $158 |
| 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | OR307223 | 25g | $545 |
| 2-Bromo-5-methylpyridine 1-oxide 95% | AS39992 | 1g | $68 |
| More product size | |||
SAFETY
Risk and Safety Statements
| Symbol(GHS) | ![]() GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| HS Code | 2933399990 |
2-broMo-5-Methylpyridine-1-o×ide price More Price(35)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR307223 | 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | 19230-58-1 | 250mg | $22 | 2026-06-04 | Buy |
| Apolloscientific | OR307223 | 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | 19230-58-1 | 1g | $49 | 2026-06-04 | Buy |
| Apolloscientific | OR307223 | 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | 19230-58-1 | 5g | $158 | 2026-06-04 | Buy |
| Apolloscientific | OR307223 | 2-Bromo-5-methylpyridin-1-ium-1-olate 98% | 19230-58-1 | 25g | $545 | 2026-06-04 | Buy |
| Activate Scientific | AS39992 | 2-Bromo-5-methylpyridine 1-oxide 95% | 19230-58-1 | 1g | $68 | 2026-06-04 | Buy |
2-broMo-5-Methylpyridine-1-o×ide Chemical Properties,Uses,Production
Synthesis
3510-66-5
19230-58-1
The general procedure for the synthesis of 2-bromo-5-methylpyridine nitrogen oxides from 2-bromo-5-methylpyridine was as follows: 2-bromo-5-methylpyridine (4 g, 2.3 mmol) was dissolved in dichloromethane (500 mL) at 0 °C and m-CPBA (52 g, 304 mmol) was added slowly. The reaction mixture was stirred continuously at room temperature for 20 hours. Upon completion of the reaction, the pH was adjusted with saturated K2CO3 solution to about 9. The organic layer was separated and concentrated to give the crude product. The crude product was purified by fast silica gel column chromatography with petroleum ether/ethyl acetate (1:1, v/v) as eluent to afford the target compound 2-bromo-5-methylpyridine 1-oxide (33 g, 75% yield). The structure of the product was confirmed by 1H NMR (CDCl3): δ 8.25 (s, 1H), 8.75 (d, 1H, J = 8.4 Hz), 6.95-6.94 (m, 1H), 2.30 (s, 3H).
References
[1] Patent: WO2011/146287, 2011, A1. Location in patent: Page/Page column 29-30
[2] Patent: WO2017/35353, 2017, A1. Location in patent: Paragraph 0911
[3] Journal of Medicinal Chemistry, 2014, vol. 57, # 16, p. 7126 - 7135
[4] Journal of Organic Chemistry, 2009, vol. 74, # 2, p. 939 - 942
2-broMo-5-Methylpyridine-1-o×ide Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Shanxi Xuanran Import and Export Trade Co., Ltd. | +8617735180244 | mike_yan@xuanranglobal.com | CHINA | 4017 | 58 |
| CR Corporation Limited | +8613062833949 | fred.wen@crcorporation.cn | China | 8645 | 58 |
| Jilin Chinese Academy of Sciences-yanshen Technology | +undefined18143011203 | info@chemextension.com | China | 42056 | 58 |
| Suzhou ARTK Medchem Co., Ltd. | +8618118463618 | sales1@artkmedchem.com | China | 39021 | 58 |
| Pure Chemistry Scientific Inc. | 001-857-928-2050 or 1-888-588-9418 | sales@chemreagents.com | United States | 10186 | 62 |
| Cool Pharm, Ltd | 021-60455363 18019463053 | sales@coolpharm.com | China | 7481 | 58 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 021-61312847; 18021002903 | 3008007409@qq.com | China | 89686 | 60 |
| Jinan Kaixi Biotechnology Co., Ltd. | 13370511208; 15853141736 | 461667177@qq.com | China | 702 | 55 |





