Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)-
- CAS No.
- 622386-94-1
- Chemical Name:
- Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)-
- Synonyms
- 4-(4-BROMOPHENYL)-1-(METHYLSULFONYL)PIPERIDINE;Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)-;Piperidine,4-(4-broMophenyl)-1-(MetChemicalbookhylsulfonyl)-
- CBNumber:
- CB52658343
- Molecular Formula:
- C12H16BrNO2S
- Molecular Weight:
- 318.23
- MDL Number:
- MFCD23701556
- MOL File:
- 622386-94-1.mol
| Product description | Number | Pack Size | Price |
| 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine | 9361AB | 10g | $371 |
| 4-(4-BROMOPHENYL)-1-(METHYLSULFONYL)PIPERIDINE 95.00% | HCH0365213 | 5MG | $502.52 |
| 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine 97% | A167921 | 250mg | $17 |
| 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine 97% | A167921 | 1g | $40 |
| 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine 95+% | CD11087671 | 10g | $236 |
| storage temp. | Sealed in dry,Room Temperature |
|---|---|
| Appearance | White to off-white Solid |
| InChI | InChI=1S/C12H16BrNO2S/c1-17(15,16)14-8-6-11(7-9-14)10-2-4-12(13)5-3-10/h2-5,11H,6-9H2,1H3 |
| InChIKey | HFRCPNHFAFLBMD-UHFFFAOYSA-N |
| SMILES | N1(S(C)(=O)=O)CCC(C2=CC=C(Br)C=C2)CC1 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)- price More Price(5)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AK Scientific | 9361AB | 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine | 622386-94-1 | 10g | $371 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0365213 | 4-(4-BROMOPHENYL)-1-(METHYLSULFONYL)PIPERIDINE 95.00% | 622386-94-1 | 5MG | $502.52 | 2021-12-16 | Buy |
| Ambeed | A167921 | 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine 97% | 622386-94-1 | 250mg | $17 | 2021-12-16 | Buy |
| Ambeed | A167921 | 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine 97% | 622386-94-1 | 1g | $40 | 2021-12-16 | Buy |
| Crysdot | CD11087671 | 4-(4-Bromophenyl)-1-(methylsulfonyl)piperidine 95+% | 622386-94-1 | 10g | $236 | 2021-12-16 | Buy |
Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)- Chemical Properties,Uses,Production
Uses
4-(4-bromophenyl)-1-(methylsulfonyl)piperidine is a piperidine derivative used in pharmaceutical synthesis and experimental research.
Synthesis
287954-99-8
622386-94-1
To the methanesulfonamide in Part A was added dichloromethane (300 mL) and triethylsilane (125 mL, 778 mmol). Trifluoroacetic acid (300 mL, 3.9 mol) was added to the suspension. The resulting mixture was stirred at ambient temperature for 1 hr while keeping the reaction vessel sealed, followed by vacuum concentration to give a solid product. The solid was mixed with methanol (150 mL) in a sealed flask at ambient temperature for 2 days. Afterwards, the solid was separated from the suspension by filtration and washed with additional methanol (100 mL). The resulting solid was dried in a vacuum oven at 50 °C overnight to yield 54.14 g (91.7% yield) of the target product 4-(4-bromophenyl)-1-(methylsulfonyl)piperidine. The structure of the product was confirmed by 1H NMR analysis.
References
[1] Patent: US2005/9838, 2005, A1. Location in patent: Page 135; 303; 308; 347
Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)- Preparation Products And Raw materials
Raw materials
Preparation Products
Piperidine,4-(4-broMophenyl)-1-(Methylsulfonyl)- Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
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| DAYANG CHEM (HANGZHOU) CO.,LTD | +86-88938639 +86-17705817739 | info@dycnchem.com | China | 53899 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
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| skychemical Co.Ltd | 021-20958197 20965099 | sales@skychemical.com | China | 1183 | 57 |
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