2-broMo-3-Methoxybenzaldehyde
- CAS No.
- 10401-18-0
- Chemical Name:
- 2-broMo-3-Methoxybenzaldehyde
- Synonyms
- 2-broMo-3-Methoxybenzaldehyde;Benzaldehyde, 2-bromo-3-methoxy-;2-Bromo-3-methoxybenzaldehyde 95%
- CBNumber:
- CB52694039
- Molecular Formula:
- C8H7BrO2
- Molecular Weight:
- 215.04
- MDL Number:
- MFCD09834663
- MOL File:
- 10401-18-0.mol
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P280-P305+P351+P338-P312 |
| HS Code | 2912490090 |
2-broMo-3-Methoxybenzaldehyde price More Price(28)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Biosynth Carbosynth | FB168551 | 2-Bromo-3-methoxybenzaldehyde | 10401-18-0 | 50mg | $100 | 2021-12-16 | Buy |
| Apolloscientific | OR400081 | 2-Bromo-3-methoxybenzaldehyde 95% | 10401-18-0 | 250mg | $131 | 2021-12-16 | Buy |
| SynQuest Laboratories | 2615-9-27 | 2-Bromo-3-methoxybenzaldehyde | 10401-18-0 | 250mg | $144 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FB168551 | 2-Bromo-3-methoxybenzaldehyde | 10401-18-0 | 100mg | $160 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FB168551 | 2-Bromo-3-methoxybenzaldehyde | 10401-18-0 | 250mg | $250 | 2021-12-16 | Buy |
2-broMo-3-Methoxybenzaldehyde Chemical Properties,Uses,Production
Synthesis
196081-71-7
74-88-4
10401-18-0
To a mixed solution of N,N-dimethylformamide (60 mL) of 2-bromo-3-hydroxybenzaldehyde (1.30 g, 6.50 mmol) and potassium carbonate (2.70 g, 19.5 mmol) was added iodomethane (0.80 g, 12.9 mmol). The reaction mixture was stirred at room temperature for 16 h. After completion of the reaction, it was diluted with ethyl acetate (60 mL). The mixture was washed with saturated aqueous ammonium chloride solution (2 x 50 mL), the organic phase was dried over anhydrous sodium sulfate and filtered. The filtrate was concentrated under reduced pressure and the residue was purified by column chromatography using a 0 to 30% ethyl acetate/hexane gradient elution to afford 2-bromo-3-methoxybenzaldehyde as a yellow oil (1.50 g, quantitative yield). Mass spectrum (electrospray positive ion mode) m/z 215.1 ([M+H]+).
References
[1] Patent: US2018/162868, 2018, A1. Location in patent: Paragraph 1413-1414
[2] Journal of the American Chemical Society, 2017, vol. 139, # 9, p. 3360 - 3363
[3] Patent: US2016/75711, 2016, A1. Location in patent: Paragraph 0586-0587
[4] Journal of Organic Chemistry, 2018, vol. 83, # 10, p. 5791 - 5800
2-broMo-3-Methoxybenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
2-broMo-3-Methoxybenzaldehyde Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Career Henan Chemica Co | +86-0371-86658258 +8613203830695 | laboratory@coreychem.com | China | 30229 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +8613336024896 | CB@aromsyn.com | China | 19183 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 | market18@leapchem.com | China | 43339 | 58 |
| Nanjing Bicbiotechnology Co., Ltd | +86-2552131256 +86-18251840740 | sales@bicbiotech.com | China | 5994 | 58 |
| Suzhou ARTK Medchem Co., Ltd. | +86-512-68323658 +86-18168183658 | sales1@artkmedchem.com | China | 39002 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Beijing Ouhe Technology Co., Ltd | 010-010-82967028 13552068683 | 2355560935@qq.com | China | 10441 | 60 |
| Adamas Reagent, Ltd. | 400-6009262 16621234537 | chenyj@titansci.com | China | 14101 | 59 |
| Bide Pharmatech Ltd. | 400-164-7117 13681763483 | product02@bidepharm.com | China | 42446 | 60 |
| Shanghai ShiXian Chemical Technology Co., Ltd. | 18681884732 | 2245256225@qq.com | China | 1737 | 50 |
