(2-Methylamino-phenyl)-methanol
- CAS No.
- 29055-08-1
- Chemical Name:
- (2-Methylamino-phenyl)-methanol
- Synonyms
- 2-(Methylamino)benzyl alcohol;o-(Methylamino)benzenemethanol;2-(Methylamino)benzenemethanol;(2-Methylamino-phenyl)-methanol;Benzenemethanol, 2-(methylamino)-
- CBNumber:
- CB5839423
- Molecular Formula:
- C8H11NO
- Molecular Weight:
- 137.18
- MDL Number:
- MFCD09031020
- MOL File:
- 29055-08-1.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
(2-Methylamino-phenyl)-methanol price More Price(28)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS101935 | 2-(Methylamino)benzenemethanol 95% | 29055-08-1 | 1g | $545 | 2026-06-04 | Buy |
| aablocks | AA002X41 | (2-(Methylamino)phenyl)methanol 95% | 29055-08-1 | 100mg | $70 | 2026-05-28 | Buy |
| aablocks | AA002X41 | (2-(Methylamino)phenyl)methanol 95% | 29055-08-1 | 250mg | $112 | 2026-05-28 | Buy |
| aablocks | AA002X41 | (2-(Methylamino)phenyl)methanol 95% | 29055-08-1 | 1g | $239 | 2026-05-28 | Buy |
| aablocks | AA002X41 | (2-(Methylamino)phenyl)methanol >95% | 29055-08-1 | 5g | $558 | 2026-05-28 | Buy |
(2-Methylamino-phenyl)-methanol Chemical Properties, Uses, Production
Synthesis
119-68-6
29055-08-1
a) Preparation of 2-(N-methylamino)benzyl alcohol Lithium aluminum hydride (0.76 g, 0.02 mol) was suspended in anhydrous tetrahydrofuran (40 mL) under argon protection. To this suspension, an anhydrous tetrahydrofuran solution of N-methylphthalamic acid (1.51 g, 0.01 mol) was slowly added. The reaction mixture was refluxed for 1 hour and then the reaction was quenched by the addition of ice water (50 mL). The mixture was filtered through a diatomaceous earth pad and the filter cake was washed thoroughly with dichloromethane (50 mL). The organic layer was separated and the aqueous layer was further extracted with dichloromethane (50 mL). All organic layers were combined, washed with brine (30 mL), dried over anhydrous sodium sulfate and concentrated under reduced pressure. The resulting pale yellow oil was purified by silica gel column chromatography (Wakogel C-200, 50 g, eluent n-hexane:ethyl acetate=2:1) to afford the colorless oil (2-(methylamino)phenyl)methanol (1.18 g, 86% yield). 1H-NMR (270 MHz, CDCl3): δ 2.87 (3H, s), 3.00-3.10 (1H, br.s), 4.64 (2H, s), 6.65-6.69 (2H, m), 7.05 (1H, d, J=7.2 Hz), 7.23-7.29 (1H, m).
References
[1] Patent: US6812238, 2004, B1. Location in patent: Page/Page column 21; 31-32
[2] Organic Letters, 2016, vol. 18, # 21, p. 5572 - 5575
(2-Methylamino-phenyl)-methanol Preparation Products And Raw materials
Raw materials
Preparation Products
(2-Methylamino-phenyl)-methanol Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Amatek Scientific Co. Ltd. | 0512-56316828 4008675858 | sales@amateksci.com | China | 9848 | 55 |
| Zhengzhou Guancheng Laboratory equipment Sales | 0371-88888888 qq272369594;2159423853qq | 2723695949@qq.com | China | 4990 | 50 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Amatek Scientific Co. Ltd. | 0512-56316828 400-867-5858;400-867-5858 | info@amateksci.com | China | 28760 | 58 |
| Aikon International Limited | 025-58859352 15955137747 | sales01@aikonchem.com | China | 16021 | 58 |
| Shanghai Amico Chemicals Co. LTD | 微信 18019252918 18019252918 | 1454668768@qq.com | China | 14933 | 58 |
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| Energy Chemical | 021-58432009 400-005-6266 | marketing@energy-chemical.com | China | 44871 | 58 |
| Hubei Co-prosperity Medicine Technonlogy Co., Ltd | 2383948258 19172820304 | 2383948258@qq.com | China | 12983 | 58 |
| Shanghai Haohong Pharmaceutical Co., Ltd. | 400-8210725 4008210725 | malulu@leyan.com | China | 39796 | 58 |
